4-Pentenoic acid, 2-oxo-2-phenylethyl ester

Base Information

Chemical Name:4-Pentenoic acid, 2-oxo-2-phenylethyl ester
CAS No.:918950-40-0
Molecular Formula:C13H14O3
Molecular Weight:218.252
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Pentenoic acid, 2-oxo-2-phenylethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
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MSDS Files:: SDS file from LookChem

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Technology Process of 4-Pentenoic acid, 2-oxo-2-phenylethyl ester

There total 1 articles about 4-Pentenoic acid, 2-oxo-2-phenylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 591-80-0
pent-4-enoic acid

: 70-11-1
α-bromoacetophenone

: 918950-40-0
pent-4-enoic acid 2-oxo-2-phenyl-ethyl ester

Guidance literature:: With Aliquat 336; sodium hydrogencarbonate; In dichloromethane; water; for 72h;
DOI:10.1021/jo061535z

Reference yield: 76.0%

: 918950-40-0
pent-4-enoic acid 2-oxo-2-phenyl-ethyl ester

: 918950-42-2
5-hydroxyphosphinoyl-pentanoic acid 2-oxo-2-phenyl-ethyl ester

Guidance literature:: With ammonium hypophosphorous acid; triethyl borane; In methanol; hexane; at 20 ℃; for 2h;
DOI:10.1021/jo061535z

Reference yield:

: 918950-40-0
pent-4-enoic acid 2-oxo-2-phenyl-ethyl ester

: 918950-46-6
5-(benzyl-hydroxy-phosphinoyl)-pentanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / NH₄H₂PO₂; triethylborane / methanol; hexane / 2 h / 20 °C

2: 71 percent / ethyldiisopropylamine; trimethylsilyl chloride / CH₂Cl₂ / 12 h / cooling

3: 96 percent / H₂ / Pd/C / methanol / 15 h / 20 °C / 760 Torr

With chloro-trimethyl-silane; ammonium hypophosphorous acid; triethyl borane; hydrogen; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In methanol; hexane; dichloromethane;
DOI:10.1021/jo061535z