5-Oxazolidinecarboxamide, N-[(1S,2R)-2-hydroxy-3-[(2-methylpropyl)[(4-nitrophenyl)sulfonyl]amino]- 1-(phenylmethyl)propyl]-2-oxo-3-phenyl-, (5S)-

Base Information

Chemical Name:5-Oxazolidinecarboxamide, N-[(1S,2R)-2-hydroxy-3-[(2-methylpropyl)[(4-nitrophenyl)sulfonyl]amino]- 1-(phenylmethyl)propyl]-2-oxo-3-phenyl-, (5S)-
CAS No.:919081-33-7
Molecular Formula:C30H34N4O8S
Molecular Weight:610.688
Hs Code.:

5-Oxazolidinecarboxamide,
N-[(1S,2R)-2-hydroxy-3-[(2-methylpropyl)[(4-nitrophenyl)sulfonyl]amino]-
1-(phenylmethyl)propyl]-2-oxo-3-phenyl-, (5S)-

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Oxazolidinecarboxamide, N-[(1S,2R)-2-hydroxy-3-[(2-methylpropyl)[(4-nitrophenyl)sulfonyl]amino]- 1-(phenylmethyl)propyl]-2-oxo-3-phenyl-, (5S)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-Oxazolidinecarboxamide, N-[(1S,2R)-2-hydroxy-3-[(2-methylpropyl)[(4-nitrophenyl)sulfonyl]amino]- 1-(phenylmethyl)propyl]-2-oxo-3-phenyl-, (5S)-

There total 8 articles about 5-Oxazolidinecarboxamide, N-[(1S,2R)-2-hydroxy-3-[(2-methylpropyl)[(4-nitrophenyl)sulfonyl]amino]- 1-(phenylmethyl)propyl]-2-oxo-3-phenyl-, (5S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1066875-99-7
2-oxo-3-phenyl-oxazolidine-5-carbonyl chloride

: 251105-80-3
N-(3S-amino-2R-hydroxy-4-phenylbutyl)-N-isobutyl-4-nitro-benzenesulfonamide hydrochloride

: 919081-33-7
2-oxo-3-phenyl-oxazolidine-5-carboxylic acid {1-benzyl-2-hydroxy-3-[isobutyl-(4-nitro-benzenesulfonyl)-amino]-propyl}-amide

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/jm060666p

Reference yield:

: 918543-49-4
(S)-2-oxo-3-phenyloxazolidine-5-carboxylic acid

: 919081-33-7
2-oxo-3-phenyl-oxazolidine-5-carboxylic acid {1-benzyl-2-hydroxy-3-[isobutyl-(4-nitro-benzenesulfonyl)-amino]-propyl}-amide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride / 20 °C

2: Et₃N / tetrahydrofuran / 20 °C

With oxalyl dichloride; triethylamine; In tetrahydrofuran;
DOI:10.1021/jm060666p

Reference yield:

: 3422-02-4
N-(benzyloxycarbonyl)aniline

: 919081-33-7
2-oxo-3-phenyl-oxazolidine-5-carboxylic acid {1-benzyl-2-hydroxy-3-[isobutyl-(4-nitro-benzenesulfonyl)-amino]-propyl}-amide

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-BuLi / tetrahydrofuran; hexane / 0.75 h / -78 °C

1.2: tetrahydrofuran; hexane / -78 - 20 °C

2.1: NaIO₄; RuCl₃*H₂O / acetonitrile; CCl₄ / 0 - 20 °C

3.1: oxalyl chloride / 20 °C

4.1: Et₃N / tetrahydrofuran / 20 °C

With ruthenium trichloride; sodium periodate; n-butyllithium; oxalyl dichloride; triethylamine; In tetrahydrofuran; tetrachloromethane; hexane; acetonitrile;
DOI:10.1021/jm060666p