Benzene, 1,1'-[2-(2,2-dimethyl-3-phenylcyclopropylidene)ethenylidene]bis-

Base Information

Chemical Name:Benzene, 1,1'-[2-(2,2-dimethyl-3-phenylcyclopropylidene)ethenylidene]bis-
CAS No.:919341-22-3
Molecular Formula:C25H22
Molecular Weight:322.45
Hs Code.:

Synonyms:

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Chemical Property of Benzene, 1,1'-[2-(2,2-dimethyl-3-phenylcyclopropylidene)ethenylidene]bis-

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Technology Process of Benzene, 1,1'-[2-(2,2-dimethyl-3-phenylcyclopropylidene)ethenylidene]bis-

There total 1 articles about Benzene, 1,1'-[2-(2,2-dimethyl-3-phenylcyclopropylidene)ethenylidene]bis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 768-49-0
(2-methyl-1-propenyl)-benzene

: 17343-74-7
1,1-dibromo-2,2-diphenylcyclopropane

: 919341-22-3
(C₆H₅)2CCCCH(C₆H₅)C(CH₃)2

Guidance literature:: With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/jo061899r

Reference yield: 98.0%

: 919341-22-3
(C₆H₅)2CCCCH(C₆H₅)C(CH₃)2

: 2-isopropyl-1,4-diphenylnaphthalene

Guidance literature:: With europium(III) trifluoroacetate; In 1,2-dichloro-ethane; at 40 ℃; for 5h;
DOI:10.1021/jo061899r

Reference yield: 68.0%

: 919341-22-3
(C₆H₅)2CCCCH(C₆H₅)C(CH₃)2

: palladium dichloride

: 1132754-37-0,1175006-96-8,1130748-25-2
(PdCl((C₆H₅)2CCC(CCH₂CH₃)CHC₆H₅))2

Guidance literature:: In tetrahydrofuran; stirring a mixt. of 1.2 equiv. PdCl2 and vinylidenecyclopropane deriv. in THF at 50°C for 12 h; evapn. in vac., flash chromy. (silica gel, CH2Cl2/petroleum ether); elem. anal.;
DOI:10.1021/om801117g