Benzenebutanenitrile, a-[(phenylmethyl)amino]-

Base Information

Chemical Name:Benzenebutanenitrile, a-[(phenylmethyl)amino]-
CAS No.:919789-43-8
Molecular Formula:C17H18N2
Molecular Weight:250.343
Hs Code.:

Synonyms:

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Chemical Property of Benzenebutanenitrile, a-[(phenylmethyl)amino]-

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Benzenebutanenitrile, a-[(phenylmethyl)amino]-

There total 6 articles about Benzenebutanenitrile, a-[(phenylmethyl)amino]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 104-53-0
3-phenyl-propionaldehyde

: 7677-24-9
trimethylsilyl cyanide

: 100-46-9
benzylamine

: 919789-43-8
2-(benzylamino)-4-phenylbutanenitrile

Guidance literature:: With mesoporous aluminosilicate Al-MCM-41; In dichloromethane; at 20 ℃; for 0.25h; Inert atmosphere;
DOI:10.1016/j.tet.2010.01.001

Reference yield:

: 501-52-0
3-Phenylpropionic acid

: 919789-43-8
2-(benzylamino)-4-phenylbutanenitrile

Guidance literature:: Multi-step reaction with 2 steps

1.1: (1,2-dimethoxyethane)dichloronickel(II); 4,4'-di-tert-butyl-2,2'-bipyridine; 2,6-dimethylpyridine; zinc; dimethyl dicarbonate / ethyl acetate / 0.25 h / Inert atmosphere; Green chemistry

1.2: 24 h / 40 °C / Inert atmosphere; Green chemistry

2.1: 1 h / Inert atmosphere

2.2: 16 h / 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; (1,2-dimethoxyethane)dichloronickel(II); 4,4'-di-tert-butyl-2,2'-bipyridine; zinc; dimethyl dicarbonate; In ethyl acetate;
DOI:10.1021/acs.orglett.9b02779

Reference yield:

: methoxycarbonyl 3-phenylpropanoate

: 919789-43-8
2-(benzylamino)-4-phenylbutanenitrile

Guidance literature:: Multi-step reaction with 2 steps

1.1: (1,2-dimethoxyethane)dichloronickel(II); 4,4'-di-tert-butyl-2,2'-bipyridine; 2,6-dimethylpyridine; zinc / ethyl acetate / 0.25 h / Inert atmosphere; Green chemistry

1.2: 24 h / 40 °C / Inert atmosphere; Green chemistry

2.1: 1 h / Inert atmosphere

2.2: 16 h / 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; (1,2-dimethoxyethane)dichloronickel(II); 4,4'-di-tert-butyl-2,2'-bipyridine; zinc; In ethyl acetate;
DOI:10.1021/acs.orglett.9b02779