Silacyclohexane, 1-(3-chloropropyl)-2-methylene-1-phenyl-

Base Information

Chemical Name:Silacyclohexane, 1-(3-chloropropyl)-2-methylene-1-phenyl-
CAS No.:919801-08-4
Molecular Formula:C15H21ClSi
Molecular Weight:264.87
Hs Code.:

Synonyms:

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Chemical Property of Silacyclohexane, 1-(3-chloropropyl)-2-methylene-1-phenyl-

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of Silacyclohexane, 1-(3-chloropropyl)-2-methylene-1-phenyl-

There total 4 articles about Silacyclohexane, 1-(3-chloropropyl)-2-methylene-1-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 87280-36-2
2,6-dibromohex-1-ene

: 3401-26-1
dichloro(3-chloropropyl)phenylsilane

: 919801-08-4
1-(3-chloropropyl)-2-methylidene-1-phenyl-1-silacylhexane

Guidance literature:: 2,6-dibromohex-1-ene; With magnesium; ethylene dibromide; In tetrahydrofuran; at 10 - 20 ℃; for 4h;

dichloro(3-chloropropyl)phenylsilane; In tetrahydrofuran; for 1.4h; Heating;
DOI:10.1016/j.jorganchem.2006.08.061

Reference yield:

: 1631-84-1
dichlorophenylsilane

: 919801-08-4
1-(3-chloropropyl)-2-methylidene-1-phenyl-1-silacylhexane

Guidance literature:: Multi-step reaction with 2 steps

1.1: 29 percent / Speier's catalyst

2.1: magnesium; 1,2-dibromoethane / tetrahydrofuran / 4 h / 10 - 20 °C

2.2: 36 percent / tetrahydrofuran / 1.4 h / Heating

With magnesium; ethylene dibromide; Speier's catalyst; In tetrahydrofuran;
DOI:10.1016/j.jorganchem.2006.08.061

Reference yield:

: 821-41-0
5-Hexen-1-ol

: 919801-08-4
1-(3-chloropropyl)-2-methylidene-1-phenyl-1-silacylhexane

Guidance literature:: Multi-step reaction with 3 steps

1.1: bromine / diethyl ether / 20 °C

2.1: potassium hydroxide / diethyl ether / Heating

2.2: NEt₃ / CH₂Cl₂ / 20 °C

2.3: LiBr / 1-methyl-pyrrolidin-2-one / 20 °C

3.1: magnesium; 1,2-dibromoethane / tetrahydrofuran / 4 h / 10 - 20 °C

3.2: 36 percent / tetrahydrofuran / 1.4 h / Heating

With potassium hydroxide; bromine; magnesium; ethylene dibromide; In tetrahydrofuran; diethyl ether;
DOI:10.1016/j.jorganchem.2006.08.061