6-Methyl-2-phenylbenzoic acid

Base Information

Chemical Name:6-Methyl-2-phenylbenzoic acid
CAS No.:92254-02-9
Molecular Formula:C14H12O2
Molecular Weight:212.248
Hs Code.:2916399090
Mol file:92254-02-9.mol

Synonyms:6-METHYL-2-PHENYLBENZOIC ACID;3-Methyl-biphenyl-2-carbonsaeure;3-methyl-biphenyl-2-carboxylic acid;3-Methyl-2-biphenylcarbonsaeure;2-phenyl-6-methylbenzoic acid;2-Methyl-6-phenylbenzoesaeure;

Suppliers and Price of 6-Methyl-2-phenylbenzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
3-Methyl-[1,1'-biphenyl]-2-carboxylicacid 95+%
5g
$ 752.00

American Custom Chemicals Corporation
3-METHYL-[1,1'-BIPHENYL]-2-CARBOXYLIC ACID 95.00%
5MG
$ 498.31

Alichem
3-Methylbiphenyl-2-carboxylicacid
250mg
$ 470.40

Alichem
3-Methylbiphenyl-2-carboxylicacid
500mg
$ 798.70

Alichem
3-Methylbiphenyl-2-carboxylicacid
1g
$ 1549.60

AK Scientific
3-Methyl-[1,1'-biphenyl]-2-carboxylicacid
5g
$ 1117.00

AK Scientific
3-Methyl-[1,1'-biphenyl]-2-carboxylicacid
1g
$ 317.00

Total 8 raw suppliers

Chemical Property of 6-Methyl-2-phenylbenzoic acid

Chemical Property:

PSA：37.30000
LogP:3.36020

Purity/Quality:

98%min ^*data from raw suppliers

3-Methyl-[1,1'-biphenyl]-2-carboxylicacid 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6-Methyl-2-phenylbenzoic acid

There total 2 articles about 6-Methyl-2-phenylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 118-90-1
ortho-methylbenzoic acid

: 108-86-1,52753-63-6
bromobenzene

: 643-93-6
3-methylbiphenyl

: 92254-02-9
3-methyl-[1,1′-biphenyl]-2-carboxylic acid

Guidance literature:: With copper(I) oxide; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; triethylphosphonium tetrafluoroborate; potassium carbonate; In 1-methyl-pyrrolidin-2-one; at 190 ℃; for 18h; Reagent/catalyst; Temperature; regioselective reaction; Inert atmosphere;
DOI:10.1002/anie.201607270

Reference yield:

: N-(2-(1H-pyrazol-1-yl)phenyl)-3-methyl-[1,1′-biphenyl]-2-carboxamide

: 74-88-4
methyl iodide

: 92254-02-9
3-methyl-[1,1′-biphenyl]-2-carboxylic acid

: N-methyl-2-(1H-pyrazol-1-yl)aniline

Guidance literature:: N-(2-(1H-pyrazol-1-yl)phenyl)-3-methyl-[1,1′-biphenyl]-2-carboxamide; With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

methyl iodide; In tetrahydrofuran; at 20 ℃; for 4h;

With sulfuric acid; In water; for 12h; Reflux;
DOI:10.1021/acs.joc.7b01883

Reference yield: 53.0%

: 92254-02-9
3-methyl-[1,1′-biphenyl]-2-carboxylic acid

: 2-methyl-6-phenylbenzoic anhydride

Guidance literature:: With potassium carbonate; p-toluenesulfonyl chloride; In dichloromethane; acetonitrile; at 20 ℃; for 48h;
DOI:10.1021/acs.joc.0c02848