2,5-Dimethoxy-4-[(E)-(4-nitrophenyl)diazenyl]benzene-1-diazonium chloride

Base Information

• Chemical Name: 2,5-Dimethoxy-4-[(E)-(4-nitrophenyl)diazenyl]benzene-1-diazonium chloride
• CAS No.: 92-34-2
• Molecular Formula: C14H12N5O4.Cl
• Molecular Weight: 349.733
• DSSTox Substance ID: DTXSID90576204
• Mol file: 92-34-2.mol

Synonyms:92-34-2;SCHEMBL1885103;DTXSID90576204;2,5-Dimethoxy-4-[(E)-(4-nitrophenyl)diazenyl]benzene-1-diazonium chloride

Chemical Property of 2,5-Dimethoxy-4-[(E)-(4-nitrophenyl)diazenyl]benzene-1-diazonium chloride

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 8
• Rotatable Bond Count: 4
• Exact Mass: 349.0577816
• Heavy Atom Count: 24
• Complexity: 477

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC(=C(C=C1N=NC2=CC=C(C=C2)[N+](=O)[O-])OC)[N+]#N.[Cl-]

Technology Process of 2,5-Dimethoxy-4-[(E)-(4-nitrophenyl)diazenyl]benzene-1-diazonium chloride

There total 1 articles about 2,5-Dimethoxy-4-[(E)-(4-nitrophenyl)diazenyl]benzene-1-diazonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C14H14N4O4 (6358-51-6) → Fast Black K salt (92-34-2)

Guidance literature:

With hydrogenchloride; sodium nitrite; In water; at 20 - 25 ℃; for 0.5h;

Reference yield: 74.0%

Fast Black K salt (92-34-2) + 2,2'-(phenylimino)bis[ethanol] (120-07-0) → 4-nitrobenzylazo-2',5'-dimethoxybenzylazo-4'''-N,N-di(2-hydroxyethyl)azobenzene

Guidance literature:

With sodium hydrogencarbonate; In methanol; water; for 1.33333h; Cooling with ice;

Reference yield: 53.0%

Fast Black K salt (92-34-2) + tert-butyl 2-((3-(methyl(phenyl)amino)propyl)amino)-2-oxoethoxycarbamate (1397243-11-6) → C31H38N8O8 (1397243-13-8)

Guidance literature:

In tetrahydrofuran; methanol; at 20 ℃;

DOI:10.1021/bc300344b

upstream raw materials:

C₁₄H₁₄N₄O₄

Downstream raw materials:

C₃₁H₃₈N₈O₈