2-Oxa-5-azabicyclo[2.2.1]heptane-5-carboxylic acid, 3-methoxy-7-(phenylmethoxy)-6-[[(tributylsilyl)oxy]methyl]-, phenylmethyl ester, (1R,3S,4S,6R,7R)-

Base Information

Chemical Name:2-Oxa-5-azabicyclo[2.2.1]heptane-5-carboxylic acid, 3-methoxy-7-(phenylmethoxy)-6-[[(tributylsilyl)oxy]methyl]-, phenylmethyl ester, (1R,3S,4S,6R,7R)-
CAS No.:927705-78-0
Molecular Formula:C34H51NO6Si
Molecular Weight:513.706
Hs Code.:

2-Oxa-5-azabicyclo[2.2.1]heptane-5-carboxylic acid,
3-methoxy-7-(phenylmethoxy)-6-[[(tributylsilyl)oxy]methyl]-, phenylmethyl
ester, (1R,3S,4S,6R,7R)-

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Chemical Property of 2-Oxa-5-azabicyclo[2.2.1]heptane-5-carboxylic acid, 3-methoxy-7-(phenylmethoxy)-6-[[(tributylsilyl)oxy]methyl]-, phenylmethyl ester, (1R,3S,4S,6R,7R)-

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Technology Process of 2-Oxa-5-azabicyclo[2.2.1]heptane-5-carboxylic acid, 3-methoxy-7-(phenylmethoxy)-6-[[(tributylsilyl)oxy]methyl]-, phenylmethyl ester, (1R,3S,4S,6R,7R)-

There total 1 articles about 2-Oxa-5-azabicyclo[2.2.1]heptane-5-carboxylic acid, 3-methoxy-7-(phenylmethoxy)-6-[[(tributylsilyl)oxy]methyl]-, phenylmethyl ester, (1R,3S,4S,6R,7R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: (1R,3R,4S,6R,7R)-7-Hydroxy-6-hydroxymethyl-3-methoxy-2-oxa-5-aza-bicyclo[2.2.1]heptane-5-carboxylic acid benzyl ester

: 98-88-4
benzoyl chloride

: 927705-78-0
(1R,3S,4S,6R,7R)-7-Benzyloxy-6-t-butyldimethylsilyloxymethyl-3-methoxy-2-oxa-5-aza-bicyclo[2.2.1]heptane-5-carboxylic acid benzyl ester

Guidance literature:: (1R,3R,4S,6R,7R)-7-Hydroxy-6-hydroxymethyl-3-methoxy-2-oxa-5-aza-bicyclo[2.2.1]heptane-5-carboxylic acid benzyl ester; With tert-butyldimethylsilyl chloride; In pyridine; at 0 ℃; for 3h;

benzoyl chloride; In pyridine; at 0 ℃; for 1h;