Methyl 2-hydroxy-3-(2-methylprop-2-en-1-yl)benzoate

Base Information

Chemical Name:Methyl 2-hydroxy-3-(2-methylprop-2-en-1-yl)benzoate
CAS No.:92847-95-5
Molecular Formula:C12H14O3
Molecular Weight:206.23800
Hs Code.:
DSSTox Substance ID:DTXSID50563453
Wikidata:Q82447896

Synonyms:92847-95-5;Methyl 2-hydroxy-3-(2-methylprop-2-en-1-yl)benzoate;methyl 2-hydroxy-3-(2-methylprop-2-enyl)benzoate;Methyl 2-hydroxy-3-(2-methylallyl)benzoate;Benzoic acid, 2-hydroxy-3-(2-methyl-2-propenyl)-, methyl ester;SCHEMBL8383960;DTXSID50563453;FCIGRPFWKHSHPU-UHFFFAOYSA-N;AKOS030615615;Methyl2-hydroxy-3-(2-methylallyl)benzoate;EN300-225936;G40910;Z1513818904;2-hydroxy-3-(2-methyl-2-propenyl) benzoic acid, methyl ester

Suppliers and Price of Methyl 2-hydroxy-3-(2-methylprop-2-en-1-yl)benzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AK Scientific
Methyl2-hydroxy-3-(2-methylprop-2-en-1-yl)benzoate
500mg
$ 409.00

Total 3 raw suppliers

Chemical Property of Methyl 2-hydroxy-3-(2-methylprop-2-en-1-yl)benzoate

Chemical Property:

Boiling Point:102-108 °C(Press: 3.0 Torr)
PSA：46.53000
Density:1.105±0.06 g/cm3(Predicted)
LogP:2.29740
XLogP3:3.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:206.094294304
Heavy Atom Count:15
Complexity:247

Purity/Quality:: Methyl2-hydroxy-3-(2-methylprop-2-en-1-yl)benzoate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=C)CC1=C(C(=CC=C1)C(=O)OC)O

Technology Process of Methyl 2-hydroxy-3-(2-methylprop-2-en-1-yl)benzoate

There total 4 articles about Methyl 2-hydroxy-3-(2-methylprop-2-en-1-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 110124-06-6
2-(2-methyl-2-propenyloxy)benzoic acid,methyl ester

: 92847-95-5
2-Hydroxy-3-(2-methyl-2-propenyl)-benzoesaeuremethylester

Guidance literature:: at 210 - 215 ℃; for 0.5h;
DOI:10.1007/BF00808952

Reference yield: 35.0%

: 140706-76-9
methyl 2-chloro-6-methyl-3-oxo-4-(2-propenyl)hept-6-enoate

: 31456-96-9
methyl 5-methyl-3-(2-propenyl)-salicylate

: 92847-95-5
2-Hydroxy-3-(2-methyl-2-propenyl)-benzoesaeuremethylester

: 140706-90-7
methyl 1-β-chloro-5-methylene-2-oxo-3β-(2-propenyl)-cyclohexane-1α-carboxylate

: 140706-91-8
methyl 3-endo-chloro-5-methyl-6-methylene-2-oxobicyclo<3.2.1>octane-3-exo-carboxylate

Guidance literature:: With copper diacetate; manganese triacetate; In acetic acid; for 14h; Yields of byproduct given; Ambient temperature;
DOI:10.1016/S0040-4020(01)92231-8

Reference yield:

: 119-36-8,8024-54-2
methyl salicylate

: 92847-95-5
2-Hydroxy-3-(2-methyl-2-propenyl)-benzoesaeuremethylester

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / acetone / Heating

2: N-methylpyrrolidinone / 7 h / Heating

With 1-methyl-pyrrolidin-2-one; potassium carbonate; In acetone;
DOI:10.1021/jm00080a016