1-(5-Bromo-1h-indol-3-yl)-2-(6-nitro-1,3-benzodioxol-5-yl)ethanone

Base Information

Chemical Name:1-(5-Bromo-1h-indol-3-yl)-2-(6-nitro-1,3-benzodioxol-5-yl)ethanone
CAS No.:93261-60-0
Molecular Formula:C₁₇H₁₁BrN₂O₅
Molecular Weight:403.189
Hs Code.:
NSC Number:105332
DSSTox Substance ID:DTXSID80295755
Wikidata:Q82035885

Synonyms:93261-60-0;1-(5-bromo-1h-indol-3-yl)-2-(6-nitro-1,3-benzodioxol-5-yl)ethanone;NSC105332;DTXSID80295755;NSC-105332

Suppliers and Price of 1-(5-Bromo-1h-indol-3-yl)-2-(6-nitro-1,3-benzodioxol-5-yl)ethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1-(5-Bromo-1h-indol-3-yl)-2-(6-nitro-1,3-benzodioxol-5-yl)ethanone

Chemical Property:

Vapor Pressure:2.14E-14mmHg at 25°C
Boiling Point:600.9°Cat760mmHg
Flash Point:317.2°C
Density:1.728g/cm³
XLogP3:3.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:401.98513
Heavy Atom Count:25
Complexity:542

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1OC2=C(O1)C=C(C(=C2)CC(=O)C3=CNC4=C3C=C(C=C4)Br)[N+](=O)[O-]

Technology Process of 1-(5-Bromo-1h-indol-3-yl)-2-(6-nitro-1,3-benzodioxol-5-yl)ethanone

There total 3 articles about 1-(5-Bromo-1h-indol-3-yl)-2-(6-nitro-1,3-benzodioxol-5-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 93329-41-0
2-benzo[1,3]dioxol-5-yl-1-(5-bromo-indol-3-yl)-ethanone

: 93261-60-0
3-<(3,4-Methylendioxy-2-nitro-phenyl)-acetyl>-5-brom-indol

Guidance literature:: With nitromethane; nitric acid;
DOI:10.1021/jo01030a515

Reference yield:

: 10075-50-0
5-bromo-1H-indole

: 93261-60-0
3-<(3,4-Methylendioxy-2-nitro-phenyl)-acetyl>-5-brom-indol

Guidance literature:: Multi-step reaction with 2 steps

1: (i) PhMgBr, benzene, Et₂O, (ii) /BRN= 177751/, (iii) aq. NaOH, EtOH

2: HNO₃, MeNO₂

With nitromethane; nitric acid;
DOI:10.1021/jo01030a515

Reference yield:

: 6845-81-4
3,4-methylenedioxyphenylacetyl chloride

: 93261-60-0
3-<(3,4-Methylendioxy-2-nitro-phenyl)-acetyl>-5-brom-indol

Guidance literature:: Multi-step reaction with 2 steps

1: (i) PhMgBr, benzene, Et₂O, (ii) /BRN= 177751/, (iii) aq. NaOH, EtOH

2: HNO₃, MeNO₂

With nitromethane; nitric acid;
DOI:10.1021/jo01030a515