Benzenebutanoic acid, a-cyano-, ethyl ester

Base Information

Chemical Name:Benzenebutanoic acid, a-cyano-, ethyl ester
CAS No.:93031-12-0
Molecular Formula:C13H15NO2
Molecular Weight:217.268
Hs Code.:

Synonyms:

Suppliers and Price of Benzenebutanoic acid, a-cyano-, ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 5 raw suppliers

Chemical Property of Benzenebutanoic acid, a-cyano-, ethyl ester

Chemical Property:

Boiling Point:163-165 °C(Press: 7 Torr)
Density:1.04 g/cm3(Temp: 29 °C)

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Benzenebutanoic acid, a-cyano-, ethyl ester

There total 2 articles about Benzenebutanoic acid, a-cyano-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 103-63-9
1-phenyl-2-bromoethane

: 105-56-6
ethyl 2-cyanoacetate

: 93031-12-0
ethyl phenethylcyanoacetate

Guidance literature:: With sodium; In ethanol; for 12h; Heating;

Reference yield:

: 122-78-1
phenylacetaldehyde

: 105-56-6
ethyl 2-cyanoacetate

: 93031-12-0
ethyl phenethylcyanoacetate

Guidance literature:: With hydrogen; ethylenediamine diacetic acid; 1-butyl-3-methylimidazolium Tetrafluoroborate; palladium on activated charcoal; at 25 ℃; for 4.5h; under 2250.18 Torr;
DOI:10.1016/j.tetlet.2005.01.092

Reference yield: 73.0%

: 104-92-7
1-bromo-4-methoxy-benzene

: 93031-12-0
ethyl phenethylcyanoacetate

: 111026-47-2
2-(4-methoxyphenyl)-4-phenylbutanenitrile

Guidance literature:: 1-bromo-4-methoxy-benzene; ethyl phenethylcyanoacetate; With C₂₂H₁₇N₃O₂; copper(I) bromide; sodium t-butanolate; In isopropyl alcohol; at 60 ℃; for 24h; Schlenk technique; Inert atmosphere;

With water; sodium hydroxide; In isopropyl alcohol; at 60 ℃; for 4h; Schlenk technique; Inert atmosphere; Cooling;
DOI:10.1002/anie.202014638