2-(4-Chlorobenzoyl)-N-phenylhydrazinecarbothioamide

Base Information

Chemical Name:2-(4-Chlorobenzoyl)-N-phenylhydrazinecarbothioamide
CAS No.:93034-60-7
Molecular Formula:C14H12ClN3OS
Molecular Weight:305.788
Hs Code.:
European Community (EC) Number:657-150-0
Nikkaji Number:J2.096.151A

Synonyms:2-(4-Chlorobenzoyl)-N-phenylhydrazinecarbothioamide;STL164010;AKOS003235470;2-[(4-chlorophenyl)carbonyl]-N-phenylhydrazinecarbothioamide

Suppliers and Price of 2-(4-Chlorobenzoyl)-N-phenylhydrazinecarbothioamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-(4-CHLOROBENZOYL)-N-PHENYLHYDRAZINECARBOTHIOAMIDE 95.00%
5MG
$ 503.82

Total 0 raw suppliers

Chemical Property of 2-(4-Chlorobenzoyl)-N-phenylhydrazinecarbothioamide

Chemical Property:

Melting Point:180-181 °C
PSA：85.25000
Density:1.393±0.06 g/cm3 (20 °C, 760 mmHg)
LogP:3.82620
XLogP3:3.3
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:305.0389609
Heavy Atom Count:20
Complexity:339

Purity/Quality:: 2-(4-CHLOROBENZOYL)-N-PHENYLHYDRAZINECARBOTHIOAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)NC(=S)NNC(=O)C2=CC=C(C=C2)Cl

Technology Process of 2-(4-Chlorobenzoyl)-N-phenylhydrazinecarbothioamide

There total 10 articles about 2-(4-Chlorobenzoyl)-N-phenylhydrazinecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 103-72-0
phenyl isothiocyanate

: 536-40-3
4-chlorobenzoic acid hydrazide

: 93034-60-7
1-[(4′-chlorophenyl)carbonyl-4-phenyl]thiosemicarbazide

Guidance literature:: In ethanol; for 4h; Heating;
DOI:10.1002/jhet.5570290512

Reference yield: 58.0%

: 122334-37-6
4-chloro-N-methoxy-N-methylbenzamide

: 5351-69-9
4-Phenyl-3-thiosemicarbazide

: 93034-60-7
1-[(4′-chlorophenyl)carbonyl-4-phenyl]thiosemicarbazide

Guidance literature:: With carbon dioxide;
DOI:10.1021/acs.joc.1c02077

Reference yield:

: 7335-27-5
ethyl 4-chlorobenzoate

: 93034-60-7
1-[(4′-chlorophenyl)carbonyl-4-phenyl]thiosemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine / ethanol; H₂O / 3 h / Heating

2: ethanol / 20 °C

With hydrazine; In ethanol; water;
DOI:10.1021/jo049088f