4-METHOXY-2-METHYLPHENYLHYDRAZINE HYDROCHLORIDE

Base Information

• Chemical Name: 4-METHOXY-2-METHYLPHENYLHYDRAZINE HYDROCHLORIDE
• CAS No.: 93048-16-9
• Molecular Formula: C₈H₁₂N₂O*ClH
• Molecular Weight: 188.657
• Mol file: 93048-16-9.mol

Synonyms:4-Methoxy-2-methylphenylhydrazine hydrochloride, 96%;

Chemical Property of 4-METHOXY-2-METHYLPHENYLHYDRAZINE HYDROCHLORIDE

Chemical Property:

• Vapor Pressure: 0.000697mmHg at 25°C
• Melting Point: 225-230oC
• Boiling Point: 303.4oC at 760 mmHg
• Flash Point: 137.3oC
• PSA: 47.28000
• LogP: 2.86450

Purity/Quality:

97% ^*data from raw suppliers

(4-Methoxy-2-methylphenyl)-hydrazine hydrochloride 95%+ ^*data from reagent suppliers

Safty Information:

• Statements: 20/21/22
• Safety Statements: 22-36/37

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-METHOXY-2-METHYLPHENYLHYDRAZINE HYDROCHLORIDE

There total 5 articles about 4-METHOXY-2-METHYLPHENYLHYDRAZINE HYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.2%

→ 7-chloro-3-methoxycarbonyl-4-oxo-1,4-dihydroquinoline-2-carbonyl chloride (179543-90-9,170143-37-0) + 1-(4-methoxy-2-methylphenyl)-hydrazine hydrochloride (93048-16-9)

Guidance literature:

Reference yield: 56.0%

SnCl2.2H2O + 2-methyl-4-methoxyaniline (102-50-1) → 1-(4-methoxy-2-methylphenyl)-hydrazine hydrochloride (93048-16-9)

Guidance literature:

With sodium nitrate; In hydrogenchloride; ethanol; water;

Reference yield: 44.0%

1-(4-methoxy-2-methylphenyl)-1,2-hydrazinedicarboxylic acid bis(2,2,2-trichloroethyl) ester (154876-10-5) → 1-(4-methoxy-2-methylphenyl)-hydrazine hydrochloride (93048-16-9)

Guidance literature:

With hydrogenchloride; ammonium acetate; zinc; 1.) MeOH, room temperature, 2.) dioxane;

DOI:10.1080/00397919708007084

upstream raw materials:

2-methyl-4-methoxyaniline

1-(4-methoxy-2-methylphenyl)-1,2-hydrazinedicarboxylic acid bis(2,2,2-trichloroethyl) ester

4-methoxy-2-methyl-aniline; hydrochloride

Downstream raw materials:

7-Chloro-4-hydroxy-2-(4-hydroxy-2-methylphenyl)-1,2,5,10-tetrahydropyridazino[4,5-b]quinoline-1,10-dione

7-Chloro-4-hydroxy-2-(4-methoxy-2-methylphenyl)-1,2,5,10-tetrahydropyridazino[4,5-b]quinoline-1,10-dione sodium salt

C₂₀H₂₀N₃O₂⁽¹⁺⁾*Cl^(1-)

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