Pyridazino[4,5-b]quinoline-1,4,10(5H)-trione, 7-chloro-2,3-dihydro-2-(4-methoxy-2-methylphenyl)-, monosodium salt

Base Information

Chemical Name:Pyridazino[4,5-b]quinoline-1,4,10(5H)-trione, 7-chloro-2,3-dihydro-2-(4-methoxy-2-methylphenyl)-, monosodium salt
CAS No.:170142-29-7
Molecular Formula:C19H14ClN3O4.Na
Molecular Weight:405.773
Hs Code.:
Mol file:170142-29-7.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Pyridazino[4,5-b]quinoline-1,4,10(5H)-trione, 7-chloro-2,3-dihydro-2-(4-methoxy-2-methylphenyl)-, monosodium salt

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of Pyridazino[4,5-b]quinoline-1,4,10(5H)-trione, 7-chloro-2,3-dihydro-2-(4-methoxy-2-methylphenyl)-, monosodium salt

There total 4 articles about Pyridazino[4,5-b]quinoline-1,4,10(5H)-trione, 7-chloro-2,3-dihydro-2-(4-methoxy-2-methylphenyl)-, monosodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 170142-20-8
7-chloro-4-hydroxy-2-(4-methoxy-2-methylphenyl)-1,2,5,10-tetrahydropyridazino[4,5-b]quinoline-1,10-dione

: 170142-29-7
7-Chloro-4-hydroxy-2-(4-methoxy-2-methylphenyl)-1,2,5,10-tetrahydropyridazino[4,5-b]quinoline-1,10-dione sodium salt

Guidance literature:: In methanol; sodium hydroxide; water;

Reference yield:

: 179543-90-9,170143-37-0
7-chloro-3-methoxycarbonyl-4-oxo-1,4-dihydroquinoline-2-carbonyl chloride

: 170142-29-7
7-Chloro-4-hydroxy-2-(4-methoxy-2-methylphenyl)-1,2,5,10-tetrahydropyridazino[4,5-b]quinoline-1,10-dione sodium salt

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; hydrazine / tetrahydrofuran; water

2: methanol; sodium hydroxide; water

With hydrogenchloride; hydrazine; In tetrahydrofuran; methanol; sodium hydroxide; water;

Reference yield:

: 102-50-1
2-methyl-4-methoxyaniline

: 170142-29-7
7-Chloro-4-hydroxy-2-(4-methoxy-2-methylphenyl)-1,2,5,10-tetrahydropyridazino[4,5-b]quinoline-1,10-dione sodium salt

Guidance literature:: Multi-step reaction with 3 steps

1: sodium nitrate / hydrogenchloride; ethanol; water

2: hydrogenchloride; hydrazine / tetrahydrofuran; water

3: methanol; sodium hydroxide; water

With hydrogenchloride; sodium nitrate; hydrazine; In tetrahydrofuran; hydrogenchloride; methanol; sodium hydroxide; ethanol; water;