O-(2-Chloro-6-fluorobenzyl)hydroxylamine hydrochloride

Base Information

• Chemical Name: O-(2-Chloro-6-fluorobenzyl)hydroxylamine hydrochloride
• CAS No.: 93081-15-3
• Molecular Formula: C₇H₇ClFNO*ClH
• Molecular Weight: 212.051
• Hs Code.: 2922199090
• DSSTox Substance ID: DTXSID50594702
• Mol file: 93081-15-3.mol

Synonyms:93081-15-3;O-(2-Chloro-6-fluorobenzyl)hydroxylamine hydrochloride;2-[(Aminooxy)methyl]-1-chloro-3-fluorobenzene hydrochloride;O-[(2-chloro-6-fluorophenyl)methyl]hydroxylamine hydrochloride;O-[(2-chloro-6-fluorophenyl)methyl]hydroxylamine;hydrochloride;2-[(Aminooxy)methyl]-1-chloro-3-fluorobenzene, HCl;O-(2-Chloro-6-fluorobenzyl)hydroxylaminehydrochloride;SCHEMBL1715797;DTXSID50594702;2-Chloro-6-Fluorobenzyloxyamine HCl;MFCD01114572;AKOS005069576;SB76778;DB-361486;CS-0316847;12E-928;2-[(Aminooxy)methyl]-1-chloro-3-fluorobenzene HCl;J-523787;Hydroxylamine, O-[(2-chloro-6-fluorophenyl)methyl]-, hydrochloride;2-[(ammoniooxy)methyl]-1-chloro-3-fluorobenzene chloride, AldrichCPR;O-[(2-Chloro-6-fluorophenyl)methyl]hydroxylamine--hydrogen chloride (1/1)

Chemical Property of O-(2-Chloro-6-fluorobenzyl)hydroxylamine hydrochloride

Chemical Property:

• Melting Point: 184～188℃
• PSA: 35.25000
• LogP: 3.37170
• Storage Temp.: Sealed in dry,Room Temperature
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 210.9966974
• Heavy Atom Count: 12
• Complexity: 125

Purity/Quality:

99% ^*data from raw suppliers

2-[(aminooxy)methyl]-1-chloro-3-fluorobenzenehydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=C(C(=C1)Cl)CON)F.Cl

Technology Process of O-(2-Chloro-6-fluorobenzyl)hydroxylamine hydrochloride

There total 1 articles about O-(2-Chloro-6-fluorobenzyl)hydroxylamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

O-(2-chloro-6-fluorobenzyl)hydroxylamine → O-(2-chloro-6-fluoro-benzyl)-hydroxylamine hydrochloride (93081-15-3)

Guidance literature:

With hydrogenchloride; In ethanol; at 0 - 5 ℃; for 72h;

DOI:10.1021/jf072733+

Reference yield:

12-oxotetradecano-14-lactam + O-(2-chloro-6-fluoro-benzyl)-hydroxylamine hydrochloride (93081-15-3) → C21H30ClFN2O2 (1003852-48-9) + C21H30ClFN2O2 (1003852-49-0)

Guidance literature:

With pyridine; for 16h;

DOI:10.1021/jf072733+

Downstream raw materials:

C₂₁H₃₀ClFN₂O₂

C₂₁H₃₀ClFN₂O₂

Refernces