1-Methyl-3-cyclohexene-1-carbaldehyde

Base Information

• Chemical Name: 1-Methyl-3-cyclohexene-1-carbaldehyde
• CAS No.: 931-96-4
• Molecular Formula: C8H12O
• Molecular Weight: 124.183
• Hs Code.: 2912299000
• Mol file: 931-96-4.mol

Synonyms:1-methyl-cyclohex-3-enecarbaldehyde;1-Methyl-1,2,3,6-tetrahydrobenzaldehyd;1-methyl-3-cyclohexene-1-carboxaldehyde;3-Cyclohexene-1-carboxaldehyde,1-methyl;1-Methyl-3-cyclohexene-1-carbaldehyde;1-Methylcyclohex-3-encarboxaldehyd;1-Methyl-cyclohex-3-encarbaldehyd;

Chemical Property of 1-Methyl-3-cyclohexene-1-carbaldehyde

Chemical Property:

• Boiling Point: 164-166 °C
• PSA: 17.07000
• Density: 0.9447 g/cm3
• LogP: 1.93170

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Methyl-3-cyclohexene-1-carbaldehyde

There total 8 articles about 1-Methyl-3-cyclohexene-1-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

2-methylpropenal (78-85-3,25120-30-3) + buta-1,3-diene (106-99-0,130983-70-9,29406-96-0,9003-17-2) → 1-methyl-3-cyclohexene-1-carboxaldehyde (931-96-4)

Guidance literature:

With 3-phenyl-propenal; bromocatecholborane; In dichloromethane; at 0 ℃; for 4h;

DOI:10.1016/S0040-4039(00)99464-4

Reference yield:

buta-1,3-diene (106-99-0,130983-70-9,29406-96-0,9003-17-2) → 1-methyl-3-cyclohexene-1-carboxaldehyde (931-96-4)

Guidance literature:

tin(IV) chloride; In benzene;

Reference yield:

2-(1-Methyl-cyclohex-3-enyl)-[1,3]dioxolane (24463-40-9) → 1-methyl-3-cyclohexene-1-carboxaldehyde (931-96-4)

Guidance literature:

With sulfuric acid; In 1,4-dioxane;

DOI:10.1021/jo00831a112

upstream raw materials:

2-methylpropenal

buta-1,3-diene

4-Methyl-4-nitrosooxymethyl-cyclohexene

2-(1-Methyl-cyclohex-3-enyl)-[1,3]dioxolane

Downstream raw materials:

4,4-dimethylcyclohexene

(1-methylcyclohexyl)methanol

1-methylcyclohexanecarbaldehyde

1-methyl-3-cyclohexenecarboxylic acid