10-Undecenoic acid, 1,2,3-propanetriyl ester

Base Information

• Chemical Name: 10-Undecenoic acid, 1,2,3-propanetriyl ester
• CAS No.: 93824-29-4
• Molecular Formula: C36H62O6
• DSSTox Substance ID: DTXSID201259646
• Nikkaji Number: J2.251.989A
• Mol file: 93824-29-4.mol

Synonyms:93824-29-4;10-Undecenoic acid, 1,2,3-propanetriyl ester;2,3-di(undec-10-enoyloxy)propyl undec-10-enoate;SCHEMBL4374215;DTXSID201259646;PD056634;1,2,3-Tri-10(Z)-Undecenoyl-rac-glycerol

Chemical Property of 10-Undecenoic acid, 1,2,3-propanetriyl ester

Chemical Property:

• XLogP3: 12.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 35
• Exact Mass: 590.45463969
• Heavy Atom Count: 42
• Complexity: 661

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C=CCCCCCCCCC(=O)OCC(COC(=O)CCCCCCCCC=C)OC(=O)CCCCCCCCC=C

Technology Process of 10-Undecenoic acid, 1,2,3-propanetriyl ester

There total 4 articles about 10-Undecenoic acid, 1,2,3-propanetriyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

10-undecenoic acid (112-38-9) + glycerol (56-81-5,25618-55-7,64333-26-2,8013-25-0) → α,β,α'-glycerol triundecenoate (93824-29-4) + α,α'-glycerol diundecenoate (1222191-67-4) + α,β-glycerol diundecenoate (1222191-68-5) + 2,3-dihydroxypropyl undec-10-enoate (62285-15-8) + β-glycerol monoundecenoate (142564-41-8)

Guidance literature:

With dodecylbenzenesulfonic acid; at 120 ℃; for 3h; Dean-Stark;

DOI:10.1007/s11746-015-2725-1

Reference yield:

1,3-Dichloro-2-propanol (96-23-1) + 10-undecenoic acid (112-38-9) → α,β,α'-glycerol triundecenoate (93824-29-4) + α,α'-glycerol diundecenoate (1222191-67-4) + α,β-glycerol diundecenoate (1222191-68-5)

Guidance literature:

10-undecenoic acid; With tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; at 100 ℃; for 24h; Inert atmosphere;

1,3-Dichloro-2-propanol; In N,N-dimethyl-formamide; toluene; Inert atmosphere;

DOI:10.1002/pola.23887

Reference yield:

10-undecenoic acid (112-38-9) + glycerol (56-81-5,25618-55-7,64333-26-2,8013-25-0) → α,β,α'-glycerol triundecenoate (93824-29-4)

Guidance literature:

With zinc; at 155 - 210 ℃; under 150 Torr; unter Einleiten von CO₂;

upstream raw materials:

10-undecenoic acid

glycerol

1,3-Dichloro-2-propanol