4-Methoxy-2-(methoxymethyl)benzaldehyde

Base Information

Chemical Name:4-Methoxy-2-(methoxymethyl)benzaldehyde
CAS No.:94527-40-9
Molecular Formula:C10H12O3
Molecular Weight:180.203
Hs Code.:
DSSTox Substance ID:DTXSID801280352
Nikkaji Number:J903.056E

Synonyms:94527-40-9;Benzaldehyde, 4-methoxy-2-(methoxymethyl)-;4-methoxy-2-(methoxymethyl)benzaldehyde;DTXSID801280352;2-(Methoxymethyl)-4-methoxybenzaldehyde

Suppliers and Price of 4-Methoxy-2-(methoxymethyl)benzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 4-Methoxy-2-(methoxymethyl)benzaldehyde

Chemical Property:

XLogP3:1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:180.078644241
Heavy Atom Count:13
Complexity:158

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COCC1=C(C=CC(=C1)OC)C=O

Technology Process of 4-Methoxy-2-(methoxymethyl)benzaldehyde

There total 3 articles about 4-Methoxy-2-(methoxymethyl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 4-Methoxy-1,2-bis-methoxymethyl-benzene

: 94527-40-9
4-methoxy-2-(methoxymethyl)benzaldehyde

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; for 3h; Ambient temperature;
DOI:10.1021/jo962172d

Reference yield: 87.0%

: 94527-39-6
1-bromo-4-methoxy-2-(methoxymethyl)benzene

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 94527-40-9
4-methoxy-2-(methoxymethyl)benzaldehyde

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1021/jo048860b

Reference yield:

: 22921-68-2
2-bromo-5-methoxy-benzoic acid

: 94527-40-9
4-methoxy-2-(methoxymethyl)benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / BH₃*THF / tetrahydrofuran / 0 - 20 °C

2: 97 percent / NaH / tetrahydrofuran / 0 - 20 °C

3: 87 percent / n-BuLi / tetrahydrofuran; hexane / -78 - 20 °C

With n-butyllithium; borane-THF; sodium hydride; In tetrahydrofuran; hexane;
DOI:10.1021/jo048860b