1,3-Dioxolan-2-one, 4-methyl-5-methylene-4-phenyl-

Base Information

Chemical Name:1,3-Dioxolan-2-one, 4-methyl-5-methylene-4-phenyl-
CAS No.:95323-23-2
Molecular Formula:C11H10O3
Molecular Weight:190.199
Hs Code.:
DSSTox Substance ID:DTXSID70472134
Nikkaji Number:J450.595F

Synonyms:95323-23-2;1,3-Dioxolan-2-one, 4-methyl-5-methylene-4-phenyl-;4-methyl-5-methylene-4-phenyl-1,3-dioxolan-2-one;SCHEMBL1694489;DTXSID70472134

Suppliers and Price of 1,3-Dioxolan-2-one, 4-methyl-5-methylene-4-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-Dioxolan-2-one, 4-methyl-5-methylene-4-phenyl-

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:190.062994177
Heavy Atom Count:14
Complexity:266

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(C(=C)OC(=O)O1)C2=CC=CC=C2

Technology Process of 1,3-Dioxolan-2-one, 4-methyl-5-methylene-4-phenyl-

There total 3 articles about 1,3-Dioxolan-2-one, 4-methyl-5-methylene-4-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 127-66-2
2-Phenyl-3-butyn-2-ol

: 124-38-9,18923-20-1
carbon dioxide

: 95323-23-2
4-methyl-5-methylidene-4-phenyl-1,3-dioxolan-2-one

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; at 25 ℃; for 10h; under 7500.75 Torr; Autoclave;
DOI:10.1039/c4cc06423b

Reference yield: 81.0%

: 127-66-2
2-Phenyl-3-butyn-2-ol

: 124-38-9,18923-20-1
carbon dioxide

: 3155-01-9
3-hydroxy-3-phenyl-butan-2-one

: 95323-23-2
4-methyl-5-methylidene-4-phenyl-1,3-dioxolan-2-one

Guidance literature:: With polystyrene-supported N-heterocyclic carbene-silver complex; at 40 ℃; for 24h; under 37503.8 Torr; Autoclave;
DOI:10.1002/adsc.201300007

Reference yield: 76.0%

: tert-butyl (2-phenylbut-3-yn-2-yl) carbonate

: 95323-23-2
4-methyl-5-methylidene-4-phenyl-1,3-dioxolan-2-one

Guidance literature:: [bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold(I); In dichloromethane; at 20 ℃; for 17h;
DOI:10.1021/ol053100o