Benzenemethanol, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-

Base Information

Chemical Name:Benzenemethanol, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-
CAS No.:96013-77-3
Molecular Formula:C13H22O2Si
Molecular Weight:238.402
Hs Code.:
European Community (EC) Number:843-743-3
DSSTox Substance ID:DTXSID10446132
Nikkaji Number:J796.238J
Mol file:96013-77-3.mol

Synonyms:96013-77-3;Benzenemethanol, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-;(3-((tert-Butyldimethylsilyl)oxy)phenyl)methanol;[3-[tert-butyl(dimethyl)silyl]oxyphenyl]methanol;{3-[(TERT-BUTYLDIMETHYLSILYL)OXY]PHENYL}METHANOL;3-(tert-Butyldimethylsilyloxy)benzyl alcohol;SCHEMBL559965;DTXSID10446132;TQR0083;SIGXMQNKJVKPQJ-UHFFFAOYSA-N;3-(tert-Butyldimethylsiloxy)benzyl alcohol;FT-0733436;EN300-302196

Suppliers and Price of Benzenemethanol, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Benzenemethanol, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-

Chemical Property:

Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:238.138906475
Heavy Atom Count:16
Complexity:221

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)(C)[Si](C)(C)OC1=CC=CC(=C1)CO

Technology Process of Benzenemethanol, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-

There total 9 articles about Benzenemethanol, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 96013-95-5
3-(tert-butyl-dimethyl-sylanyloxy)benzaldehyde

: 96013-77-3
3-(tert-butyldimethylsilyloxy)benzyl alcohol

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 ℃; for 0.166667h;
DOI:10.1248/cpb.45.939

Reference yield: 98.0%

: 96013-69-3
tert-butyl((3-((tert-butyldimethylsilyl)oxy)benzyl)oxy)dimethylsilane

: 96013-77-3
3-(tert-butyldimethylsilyloxy)benzyl alcohol

Guidance literature:: With hydrogen fluoride; In acetonitrile; for 0.5h;
DOI:10.1016/S0040-4039(00)89178-9

Reference yield: 96.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 100-83-4
meta-hydroxybenzaldehyde

: 96013-77-3
3-(tert-butyldimethylsilyloxy)benzyl alcohol

Guidance literature:: tert-butyldimethylsilyl chloride; meta-hydroxybenzaldehyde; With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; for 15h;

With sodium tetrahydroborate; In methanol; dichloromethane; at 0 - 20 ℃; for 2.25h;
DOI:10.1002/anie.201604921