3,3-Bis(4-chlorophenyl)prop-2-en-1-ol

Base Information

Chemical Name:3,3-Bis(4-chlorophenyl)prop-2-en-1-ol
CAS No.:96089-74-6
Molecular Formula:C15H12Cl2O
Molecular Weight:279.166
Hs Code.:
DSSTox Substance ID:DTXSID20607090
Nikkaji Number:J2.047.662A

Synonyms:96089-74-6;3,3-Bis(4-chlorophenyl)prop-2-en-1-ol;SCHEMBL9052487;DTXSID20607090;DB-112349

Suppliers and Price of 3,3-Bis(4-chlorophenyl)prop-2-en-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,3-Bis(4-chlorophenyl)prop-2-en-1-ol

Chemical Property:

PSA：20.23000
LogP:4.41740
XLogP3:4.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:278.0265204
Heavy Atom Count:18
Complexity:250

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1C(=CCO)C2=CC=C(C=C2)Cl)Cl

Technology Process of 3,3-Bis(4-chlorophenyl)prop-2-en-1-ol

There total 4 articles about 3,3-Bis(4-chlorophenyl)prop-2-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 95269-22-0,133262-95-0
ethyl 3,3-bis(4'-chlorophenyl)prop-2-enoate

: 96089-74-6
3,3-bis-(4-chlorophenyl)prop-2-en-1-ol

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; toluene; at -20 ℃; for 1.25h;

Reference yield: 42.0%

: 1102376-68-0
2,2-bis(4-chlorophenyl)oxetane

: 1102376-72-6
3,3-bis-(4-chlorophenyl)propan-1-ol

: 96089-74-6
3,3-bis-(4-chlorophenyl)prop-2-en-1-ol

Guidance literature:: 2,2-bis(4-chlorophenyl)oxetane; With 2,4,6-trimethyl-pyridine; bis(cyclopentadienyl)titanium dichloride; manganese; chloro-trimethyl-silane; In tetrahydrofuran; at 60 ℃; Inert atmosphere;

With hydrogenchloride; water; In tetrahydrofuran; Inert atmosphere;
DOI:10.1016/j.tet.2008.08.107

Reference yield:

: 90-98-2
4,4'-Dichlorobenzophenone

: 96089-74-6
3,3-bis-(4-chlorophenyl)prop-2-en-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / toluene / 0.5 h / 4 °C

1.2: 84 percent / toluene / 20 °C

2.1: 99 percent / DibAl-H / toluene / 1 h / -5 - 20 °C

With sodium hydride; diisobutylaluminium hydride; In toluene; 1.1: Horner-Emmons reaction;
DOI:10.1016/S0968-0896(01)00436-9