Ethyl 3,3-bis(4-chlorophenyl)prop-2-enoate

Base Information

Chemical Name:Ethyl 3,3-bis(4-chlorophenyl)prop-2-enoate
CAS No.:95269-22-0
Molecular Formula:C₁₇H₁₄Cl₂O₂
Molecular Weight:321.203
Hs Code.:
DSSTox Substance ID:DTXSID10542401
Nikkaji Number:J1.678.451F

Synonyms:95269-22-0;Ethyl 3,3-bis(4-chlorophenyl)prop-2-enoate;SCHEMBL3268819;DTXSID10542401

Suppliers and Price of Ethyl 3,3-bis(4-chlorophenyl)prop-2-enoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethyl 3,3-bis(4-chlorophenyl)prop-2-enoate

Chemical Property:

XLogP3:5.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:320.0370851
Heavy Atom Count:21
Complexity:341

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOC(=O)C=C(C1=CC=C(C=C1)Cl)C2=CC=C(C=C2)Cl

Technology Process of Ethyl 3,3-bis(4-chlorophenyl)prop-2-enoate

There total 8 articles about Ethyl 3,3-bis(4-chlorophenyl)prop-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 637-87-6
1-Chloro-4-iodobenzene

: 140-88-5,9003-32-1
ethyl acrylate

: 95269-22-0,133262-95-0
ethyl 3,3-bis(4'-chlorophenyl)prop-2-enoate

Guidance literature:: With silver(I) acetate; palladium diacetate; acetic acid; at 110 ℃; for 6h;
DOI:10.1016/j.tet.2011.12.017

Reference yield: 87.0%

: 106-39-8
bromochlorobenzene

: 140-88-5,9003-32-1
ethyl acrylate

: 95269-22-0,133262-95-0
ethyl 3,3-bis(4'-chlorophenyl)prop-2-enoate

Guidance literature:: With dipalladium(II)(1,1'-di-t-butyl-3,3'-(1,2-ethanediyl)bisimidazolium)dipyridinetetradichloride; tetrabutylammomium bromide; sodium acetate; In N,N-dimethyl acetamide; at 120 ℃; for 18h; Reagent/catalyst; Catalytic behavior; Inert atmosphere; Schlenk technique;
DOI:10.1002/zaac.201200425

Reference yield: 84.0%

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 90-98-2
4,4'-Dichlorobenzophenone

: 95269-22-0,133262-95-0
ethyl 3,3-bis(4'-chlorophenyl)prop-2-enoate

Guidance literature:: diethoxyphosphoryl-acetic acid ethyl ester; With sodium hydride; In toluene; at 4 ℃; for 0.5h;

4,4'-Dichlorobenzophenone; In toluene; at 4 - 20 ℃;
DOI:10.1016/S0968-0896(03)00373-0