Silanamine, 1-(1,1-dimethylethyl)-1,1-dimethyl-N-(phenylmethyl)-

Base Information

Chemical Name:Silanamine, 1-(1,1-dimethylethyl)-1,1-dimethyl-N-(phenylmethyl)-
CAS No.:96201-10-4
Molecular Formula:C13H23NSi
Molecular Weight:221.418
Hs Code.:
DSSTox Substance ID:DTXSID70476551
Nikkaji Number:J1.967.446K
Wikidata:Q82308033

Synonyms:Silanamine, 1-(1,1-dimethylethyl)-1,1-dimethyl-N-(phenylmethyl)-;96201-10-4;DTXSID70476551;PCVGNYJCORRBMN-UHFFFAOYSA-N;Benzylamine, N-tert-butyldimethylsilyl-;Benzyl(tert-butyldimethylsilyl)amine

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Silanamine, 1-(1,1-dimethylethyl)-1,1-dimethyl-N-(phenylmethyl)-

Chemical Property:

Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:221.159976272
Heavy Atom Count:15
Complexity:187

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)[Si](C)(C)NCC1=CC=CC=C1

Technology Process of Silanamine, 1-(1,1-dimethylethyl)-1,1-dimethyl-N-(phenylmethyl)-

There total 2 articles about Silanamine, 1-(1,1-dimethylethyl)-1,1-dimethyl-N-(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 29681-57-0
tert-butyldimethylsilane

: 100-46-9
benzylamine

: 96201-10-4
benzyl(tert-butyldimethylsilyl)amine

Guidance literature:: palladium on activated charcoal; In benzene; at 70 ℃; for 1.5h;
DOI:10.1246/bcsj.62.2111

Reference yield: 99.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 100-46-9
benzylamine

: 96201-10-4
benzyl(tert-butyldimethylsilyl)amine

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In benzene; for 1.5h; Ambient temperature;
DOI:10.1016/S0040-4039(00)61915-9

Reference yield: 55.0%

: 96201-10-4
benzyl(tert-butyldimethylsilyl)amine

: 7699-45-8
zinc dibromide

: zinc bis[(benzyl)(tert-butyldimethylsilyl)amide]

Guidance literature:: With n-BuLi; In hexane; pentane; byproducts: C4H10, LiBr; Ar; addn. of n-BuLi soln. in hexane to amine in pentane at -78°, warming-up, stirring at room temp. for 8 h, crystn. at -18°C, decantation, solid was dissolved in pentane at 0°C, addn. of ZnBr2, stirring at room temp. for several d; pptn., concn. of soln. to oily residue, crystn. at -18°C; elem. anal.;