Technology Process of Diphenylbis(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)stannane
There total 1 articles about Diphenylbis(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)stannane which
guide to synthetic route it.
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synthetic route:
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76598-01-1
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl magnesium iodide
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96325-94-9
(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)2SnPh2
- Guidance literature:
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In
diethyl ether;
byproducts: (CF3(CF2)5CH2CH2)2; a soln. of Sn-compound added to a soln. of Grignard compound; hydrolyzed with NH4Cl soln.; washed with 5% Na2S2O3 soln. and water; dried; evapd.; chromy.;
DOI:10.1002/bscb.19840931209
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96325-94-9
(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)2SnPh2
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96325-95-0
(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)2SnPhCl
- Guidance literature:
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With
chlorine;
In
methanol;
byproducts: chlorobenzene; an ice-cooled suspn. of Sn-compound titrated with a soln. of Cl2; evapd.; recrystd. from n-hexane;
DOI:10.1002/bscb.19840931209