3-(Benzyloxy)-2-bromo-5-methoxybenzaldehyde

Base Information

Chemical Name:3-(Benzyloxy)-2-bromo-5-methoxybenzaldehyde
CAS No.:97227-88-8
Molecular Formula:C15H13BrO3
Molecular Weight:321.17
Hs Code.:
DSSTox Substance ID:DTXSID40568634
Wikidata:Q82454947

Synonyms:3-(Benzyloxy)-2-bromo-5-methoxybenzaldehyde;97227-88-8;SCHEMBL13744497;DTXSID40568634

Suppliers and Price of 3-(Benzyloxy)-2-bromo-5-methoxybenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(Benzyloxy)-2-bromo-5-methoxybenzaldehyde

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:320.00481
Heavy Atom Count:19
Complexity:279

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=C(C(=C1)OCC2=CC=CC=C2)Br)C=O

Technology Process of 3-(Benzyloxy)-2-bromo-5-methoxybenzaldehyde

There total 2 articles about 3-(Benzyloxy)-2-bromo-5-methoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 100-39-0
benzyl bromide

: 108791-60-2
2-bromo-3-hydroxy-5-methoxybenzaldehyde

: 97227-88-8
3-(benzyloxy)-2-bromo-5-methoxybenzaldehyde

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 22h;

Reference yield:

: 139077-39-7
3-methoxy-5-methylphenyl acetate

: 97227-88-8
3-(benzyloxy)-2-bromo-5-methoxybenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / N-bromosuccinimide (NBS), benzoyl peroxide / CCl₄ / 72 h / Heating

2: 100 percent / ammonium formate, water / ethanol / 24 h / Heating

3: 66 percent / potassium carbonate / dimethylformamide / 22 h

With N-Bromosuccinimide; Perbenzoic acid; water; ammonium formate; potassium carbonate; In tetrachloromethane; ethanol; N,N-dimethyl-formamide;