Boc-2,6-diaminopimelic acid

Base Information

• Chemical Name: Boc-2,6-diaminopimelic acid
• CAS No.: 98469-29-5
• Molecular Formula: C₁₇H₃₀N₂O₈
• Molecular Weight: 390.434
• Hs Code.: 2922499990
• Mol file: 98469-29-5.mol

Synonyms:Heptanedioic acid,2,6-bis[[(1,1-dimethylethoxy)carbonyl]amino];2,6-bis[(tert-butoxycarbonyl)amino]heptanedioic acid;

Chemical Property of Boc-2,6-diaminopimelic acid

Chemical Property:

• PSA: 151.26000
• LogP: 2.89430

Purity/Quality:

98%min ^*data from raw suppliers

Di-Boc-2,6-diaminoheptanedioic acid (mixture ofisomers) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Boc-2,6-diaminopimelic acid

There total 2 articles about Boc-2,6-diaminopimelic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

di-tert-butyl dicarbonate (24424-99-5) + (+/-)-2,6-Diaminopimelic acid (583-93-7,922-54-3,2577-62-0,14289-34-0,17121-19-6,1356383-43-1) → C17H30N2O8 (98469-29-5)

Guidance literature:

With sodium carbonate; In 1,4-dioxane; water; at 0 - 20 ℃;

DOI:10.2174/092986610790780387

Reference yield:

2,6-diaminopimelic acid (922-54-3,2577-62-0,14289-34-0,17121-19-6,583-93-7,1356383-43-1) + di-tert-butyl dicarbonate (24424-99-5) → C17H30N2O8 (98469-29-5)

Guidance literature:

With triethylamine; In water; for 6h;

DOI:10.1021/jm101535e

Reference yield: 83.0%

C17H30N2O8 (98469-29-5) + O-benzyl-N,N'-diisopropylisourea (2978-10-1) → dibenzyl 2,6-bis((tert-butoxycarbonyl)amino)heptanedioate (1227363-56-5)

Guidance literature:

In N,N-dimethyl-formamide; benzene; at 80 ℃; for 8h;

DOI:10.2174/092986610790780387

upstream raw materials:

2,6-diaminopimelic acid

di-tert-butyl dicarbonate

(+/-)-2,6-Diaminopimelic acid

Downstream raw materials:

C₁₁H₂₂N₂O₄*ClH

(5R)-tribenzyl 1-(9H-fluoren-9-yl)-18,18-dimethyl-3,8,16-trioxo-2,17-dioxa-4,9,15-triazanonadecane-5,10,14-tricarboxylate

(5R)-5-allyl 10,14-dibenzyl-1-(9H-fluoren-9-yl)-18,18-dimethyl-3,8,16-trioxo-2,17-dioxa-4,9,15-triazanonadecane-5,10,14-tricarboxylate

(5R)-5-benzyl 10,14-diethyl-1-(9H-fluoren-9-yl)-18,18-dimethyl-3,8,16-trioxo-2,17-dioxa-4,9,15-triazanonadecane-5,10,14-tricarboxylate

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