Benzenamine, N-[[2-(diphenylphosphino)phenyl]methylene]-

Base Information

Chemical Name:Benzenamine, N-[[2-(diphenylphosphino)phenyl]methylene]-
CAS No.:98821-90-0
Molecular Formula:C25H20NP
Molecular Weight:365.414
Hs Code.:
DSSTox Substance ID:DTXSID10411901
Nikkaji Number:J895.966H

Synonyms:Benzenamine, N-[[2-(diphenylphosphino)phenyl]methylene]-;98821-90-0;DTXSID10411901;N-(2-(diphenylphosphino)benzylidene)aniline

Suppliers and Price of Benzenamine, N-[[2-(diphenylphosphino)phenyl]methylene]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenamine, N-[[2-(diphenylphosphino)phenyl]methylene]-

Chemical Property:

XLogP3:6.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:5
Exact Mass:365.133336640
Heavy Atom Count:27
Complexity:425

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)N=CC2=CC=CC=C2P(C3=CC=CC=C3)C4=CC=CC=C4

Technology Process of Benzenamine, N-[[2-(diphenylphosphino)phenyl]methylene]-

There total 2 articles about Benzenamine, N-[[2-(diphenylphosphino)phenyl]methylene]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 50777-76-9
(2-formylphenyl)(diphenyl)phosphine

: 62-53-3
aniline

: 98821-90-0
N-(2-(diphenylphosphino)phenyl)methylene benzenamine

Guidance literature:: In toluene; for 19h; Heating;
DOI:10.1016/S0022-328X(02)02153-8

Reference yield: 90.0%

: 50777-76-9
(2-formylphenyl)(diphenyl)phosphine

: 100-52-7
benzaldehyde

: 98821-90-0
N-(2-(diphenylphosphino)phenyl)methylene benzenamine

Guidance literature:: In methanol; at 20 ℃;
DOI:10.1039/b109290a

Reference yield: 90.0%

: 15529-49-4,41756-81-4
tris(triphenylphosphine)ruthenium(II) chloride

: 98821-90-0
N-(2-(diphenylphosphino)phenyl)methylene benzenamine

: 540772-38-1
[RuCl2(κ²-P,N-2-Ph2PC6H4CH=NPh)(PPh3)]

Guidance literature:: In tetrahydrofuran; under dry N2, Schlenk technique; stirring for 2 h at room temp.; soln. was evapd. to dryness, residue was washed 3 times with hexane/Et2O; elem. anal. (two non-septd. isomers);
DOI:10.1039/b206119h