12-Bromododec-1-ene

Base Information

Chemical Name:12-Bromododec-1-ene
CAS No.:99828-63-4
Molecular Formula:C12H23Br
Molecular Weight:247.219
Hs Code.:
DSSTox Substance ID:DTXSID60450981
Nikkaji Number:J1.920.112K
Wikidata:Q82270823
Mol file:99828-63-4.mol

Synonyms:12-bromododec-1-ene;99828-63-4;1-Dodecene, 12-bromo-;12-Bromo-1-dodecene;12-bromododecene;SCHEMBL5405862;DTXSID60450981;ZIGYFXNWSWECFA-UHFFFAOYSA-N;AMY27230;ZDA82863;MFCD28125802;AKOS025146521;CS-W005954;BS-22326;A852533

Suppliers and Price of 12-Bromododec-1-ene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
12-Bromododec-1-ene 95+%
1g
$ 200.00

Ambeed
12-Bromododec-1-ene 98%
1g
$ 270.00

Ambeed
12-Bromododec-1-ene 98%
250mg
$ 108.00

Ambeed
12-Bromododec-1-ene 98%
5g
$ 806.00

Abosyn
12-Bromododec-1-ene 95%-98%
1g
$ 450.00

Total 18 raw suppliers

Chemical Property of 12-Bromododec-1-ene

Chemical Property:

Boiling Point:270.2±9.0 °C(Predicted)
PSA：0.00000
Density:1.052±0.06 g/cm3(Predicted)
LogP:5.07820
XLogP3:6.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:10
Exact Mass:246.09831
Heavy Atom Count:13
Complexity:99.3

Purity/Quality:

99%, ^*data from raw suppliers

12-Bromododec-1-ene 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CCCCCCCCCCCBr

Technology Process of 12-Bromododec-1-ene

There total 2 articles about 12-Bromododec-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 5876-87-9
1,11-dodecadiene

: 3344-70-5
1,12-dibromododecane

: 99828-63-4
dodec-11-ene bromide

Guidance literature:: With 2,2,4-trimethylpentane; tetradecafluorohexane; bromine; at 20 ℃; for 2h; Irradiation;
DOI:10.1055/s-0030-1258482

Reference yield:

: 55362-80-6
9-bromononan-1-ol

: 99828-63-4
dodec-11-ene bromide

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene-4-sulfonic acid / dichloromethane / 5 h / 0 - 20 °C

2.1: iodine; magnesium / tetrahydrofuran / 5.33 h / 20 °C / Inert atmosphere; Reflux

2.2: 12 h / 20 - 80 °C / Ionic liquid

3.1: pyridinium p-toluenesulfonate / methanol / 50 °C

4.1: triphenylphosphine; carbon tetrabromide / dichloromethane / -10 °C

With carbon tetrabromide; iodine; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; magnesium; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.3390/molecules18055201