Isopropyl dodec-11-enylfluorophosphonate

Base Information

Chemical Name:Isopropyl dodec-11-enylfluorophosphonate
CAS No.:623114-64-7
Molecular Formula:C15H30FO2P
Molecular Weight:292.37
Hs Code.:
Mol file:623114-64-7.mol

Synonyms:Isopropyl dodec-11-enylfluorophosphonate;Isopropyl dodec-11-enylfluorophosphonate Exclusive

Suppliers and Price of Isopropyl dodec-11-enylfluorophosphonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Cayman Chemical
Isopropyl dodec-11-enylfluorophosphonate ≥98%
10mg
$ 784.00

Cayman Chemical
Isopropyl dodec-11-enylfluorophosphonate ≥98%
5mg
$ 448.00

Cayman Chemical
Isopropyl dodec-11-enylfluorophosphonate ≥98%
1mg
$ 191.00

Cayman Chemical
Isopropyl dodec-11-enylfluorophosphonate ≥98%
500μg
$ 101.00

AK Scientific
12-[Fluoro(propan-2-yloxy)phosphoryl]dodec-1-ene
10mg
$ 1158.00

Total 12 raw suppliers

Chemical Property of Isopropyl dodec-11-enylfluorophosphonate

Chemical Property:

Boiling Point:351.5±11.0 °C(Predicted)
PSA：36.11000
Density:0.950±0.06 g/cm3(Predicted)
LogP:6.27090

Purity/Quality:

≥98% ^*data from raw suppliers

Isopropyl dodec-11-enylfluorophosphonate ≥98% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Isopropyl dodec-11-enylfluorophosphonate

There total 6 articles about Isopropyl dodec-11-enylfluorophosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 67-63-0,8013-70-5
isopropyl alcohol

: 623114-63-6
dodec-11-enyldifluorophosphonate

: 623114-64-7
isopropyl dodec-11-enylfluorophosphonate

Guidance literature:: With triethylamine; In diethyl ether; at 0 ℃; for 1h;
DOI:10.1081/SCC-120021043

Reference yield:

: 3344-70-5
1,12-dibromododecane

: 623114-64-7
isopropyl dodec-11-enylfluorophosphonate

Guidance literature:: Multi-step reaction with 6 steps

1.1: 33 percent / (i-C₃H₇)2NLi / tetrahydrofuran / 6 h / -20 - 20 °C

2.1: NaH / tetrahydrofuran / 0 - 20 °C

2.2: 80 percent / tetrahydrofuran / Heating

3.1: CH₂Cl₂ / 1.5 h / 0 - 20 °C

4.1: H₂O / acetone / 1 h / 20 °C

5.1: 99 percent / (CH₃)2NSF₃ / CHCl₃ / 0.33 h / 0 - 20 °C

6.1: 96 percent / Et₃N / diethyl ether / 1 h / 0 °C

With dimethylaminosulphur trifluoride; water; sodium hydride; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane; chloroform; acetone;
DOI:10.1081/SCC-120021043

Reference yield:

: 99828-63-4
dodec-11-ene bromide

: 623114-64-7
isopropyl dodec-11-enylfluorophosphonate

Guidance literature:: Multi-step reaction with 5 steps

1.1: NaH / tetrahydrofuran / 0 - 20 °C

1.2: 80 percent / tetrahydrofuran / Heating

2.1: CH₂Cl₂ / 1.5 h / 0 - 20 °C

3.1: H₂O / acetone / 1 h / 20 °C

4.1: 99 percent / (CH₃)2NSF₃ / CHCl₃ / 0.33 h / 0 - 20 °C

5.1: 96 percent / Et₃N / diethyl ether / 1 h / 0 °C

With dimethylaminosulphur trifluoride; water; sodium hydride; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane; chloroform; acetone;
DOI:10.1081/SCC-120021043