1,3-dihydrospiro[indene-2,4'-piperidine]-1-one

Base Information

• Chemical Name: 1,3-dihydrospiro[indene-2,4'-piperidine]-1-one
• CAS No.: 185525-49-9
• Molecular Formula: C13H15NO.ClH
• Molecular Weight: 201.2643
• Hs Code.: 2933399090
• Mol file: 185525-49-9.mol

Synonyms:SPIRO[INDENE-2,4-PIPERIDIN]-1(3H)-ONE HCL;1,3-dihydrospiro[indene-2,4'-piperidine]-1-one;Spiro[indene-2,4-piperidin]-1(3H)-one hydrochloride;Spiro[Indene-2,4'-piperidin]-1(3h)-one Hydrochloric Acid Salt

Chemical Property of 1,3-dihydrospiro[indene-2,4'-piperidine]-1-one

Chemical Property:

• PSA: 29.10000
• LogP: 2.92600

Purity/Quality:

99%, ^*data from raw suppliers

Spiro[indene-2,4''-piperidin]-1(3H)-onehydrochloride 96% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3-dihydrospiro[indene-2,4'-piperidine]-1-one

There total 1 articles about 1,3-dihydrospiro[indene-2,4'-piperidine]-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

tert-butyl 1-oxo-1,3-dihydrospiro[indene-2,4’-piperidine]-1’-carboxylate (1228079-29-5) → spiro[indene-2,4’-piperidin]-1(3H)-one hydrochloride salt (185525-49-9)

Guidance literature:

With hydrogenchloride; water; In 1,4-dioxane; at 20 ℃;

DOI:10.1016/j.bmcl.2009.11.043

Reference yield:

spiro[indene-2,4’-piperidin]-1(3H)-one hydrochloride salt (185525-49-9) + C13H12ClN3O2 (1024604-75-8) → C26H26N4O3 (1207163-36-7)

Guidance literature:

In butan-1-ol; at 100 ℃;

DOI:10.1016/j.bmcl.2009.11.043

upstream raw materials:

tert-butyl 1-oxo-1,3-dihydrospiro[indene-2,4’-piperidine]-1’-carboxylate

Downstream raw materials:

C₂₆H₂₆N₄O₃

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