9-Butyl-9H-carbazole-3-carbaldehyde

Base Information

Chemical Name:9-Butyl-9H-carbazole-3-carbaldehyde
CAS No.:67707-09-9
Molecular Formula:C17H17NO
Molecular Weight:251.328
Hs Code.:
European Community (EC) Number:266-958-9
DSSTox Substance ID:DTXSID30987052
Nikkaji Number:J333.322A
Wikidata:Q82975206
Mol file:67707-09-9.mol

Synonyms:9-Butyl-9H-carbazole-3-carbaldehyde;67707-09-9;EINECS 266-958-9;9-butylcarbazole-3-carbaldehyde;3-formyl-9-butylcarbazole;SCHEMBL9019646;DTXSID30987052;W-111292

Suppliers and Price of 9-Butyl-9H-carbazole-3-carbaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 8 raw suppliers

Chemical Property of 9-Butyl-9H-carbazole-3-carbaldehyde

Chemical Property:

Vapor Pressure:8.39E-06mmHg at 25°C
Boiling Point:374.4°Cat760mmHg
Flash Point:180.2°C
PSA：22.00000
Density:1.1g/cm³
LogP:4.40710
XLogP3:4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:251.131014166
Heavy Atom Count:19
Complexity:316

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCN1C2=C(C=C(C=C2)C=O)C3=CC=CC=C31

Technology Process of 9-Butyl-9H-carbazole-3-carbaldehyde

There total 6 articles about 9-Butyl-9H-carbazole-3-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1484-08-8
9-butyl-9H-carbazole

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 67707-09-9
9-butyl-9H-carbazole-3-carbaldehyde

Guidance literature:: N,N-dimethyl-formamide; With trichlorophosphate; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 1h; Inert atmosphere;

9-butyl-9H-carbazole; In N,N-dimethyl-formamide; at 100 ℃; for 1h; Inert atmosphere; Microwave irradiation;
DOI:10.1016/j.ejmech.2013.09.038

Reference yield:

: 86-74-8,105184-46-1,97960-57-1
9H-carbazole

: 67707-09-9
9-butyl-9H-carbazole-3-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide / water; acetone / 12 h / Reflux

2: trichlorophosphate / chlorobenzene / 5 h / 65 - 70 °C

With N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide; trichlorophosphate; In water; chlorobenzene; acetone; 2: Vilsmeier-Haack reaction / 2: Vilsmeier-Haack reaction;
DOI:10.1134/S1070428011040117