2,2'-(7H-purin-6-ylazanediyl)diethanol

Base Information

• Chemical Name: 2,2'-(7H-purin-6-ylazanediyl)diethanol
• CAS No.: 6312-66-9
• Molecular Formula: C9H13N5O2
• Molecular Weight: 223.2318
• Mol file: 6312-66-9.mol

Synonyms:Bis-(2-hydroxy-aethyl)-(7(9)H-purin-6-yl)-amin;bis-(2-hydroxy-ethyl)-(7(9)H-purin-6-yl)-amine;6-((N,N-di-2-hydroxyethyl)amino)purine;6- purin;2,2'-(7(9)H-purin-6-ylazanediyl)-bis-ethanol;2-[(2-hydroxyethyl)(9H-purin-6-yl)amino]ethan-1-ol;

Chemical Property of 2,2'-(7H-purin-6-ylazanediyl)diethanol

Chemical Property:

• Boiling Point: 429.8°Cat760mmHg
• Flash Point: 213.8°C
• PSA: 98.16000
• Density: 1.54g/cm³
• LogP: -0.85610

Purity/Quality:

99% ^*data from raw suppliers

6-(BIS-(2-HYDROXYETHYL)AMINO)PURINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,2'-(7H-purin-6-ylazanediyl)diethanol

There total 6 articles about 2,2'-(7H-purin-6-ylazanediyl)diethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2,2'-iminobis[ethanol] (111-42-2) + 6-chloropurine (87-42-3) → 2,2'--diethanol (6312-66-9)

Guidance literature:

In water; at 100 ℃; for 0.166667h; Microwave irradiation;

DOI:10.1039/b902025j

Reference yield: 84.0%

2,2'-iminobis[ethanol] (111-42-2) + 6-chloropurine (87-42-3) → 6- purin (6312-66-9)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 80 ℃; for 0.833333h; Microwave irradiation;

DOI:10.1080/15257770.2013.763977

Reference yield:

6-chloro-7H-purine (87-42-3,111055-92-6) + 2,2'-iminobis[ethanol] (111-42-2) → 6- purin (6312-66-9)

Guidance literature:

upstream raw materials:

(7⁽⁹⁾H-purin-6-ylsulfanyl)-acetic acid

2,2'-iminobis[ethanol]

6-chloro-7H-purine

6-chloropurine

Refernces

• 1、 Qu, Gui-Rong,Wu, Jing,Wu, Yan-Yan,Zhang, Feng,Guo, Hai-Ming. "Synthesis of novel 6-[N,N-bis(2-hydroxyethyl)amino]purine nucleosides under microwave irradiation in neat water". supporting information; experimental part. p. 760 - 762. Retrieved 2010/04/23.