Benzeneacetamide, 2,4-dichloro-N-(4-chlorophenyl)-a-methylene-

Base Information

Chemical Name:Benzeneacetamide, 2,4-dichloro-N-(4-chlorophenyl)-a-methylene-
CAS No.:108664-50-2
Molecular Formula:C15H10 Cl3 N O
Molecular Weight:326.605
Hs Code.:
DSSTox Substance ID:DTXSID40148697
Wikidata:Q83014294
ChEMBL ID:CHEMBL37715

Synonyms:108664-50-2;Benzeneacetamide, 2,4-dichloro-N-(4-chlorophenyl)-a-methylene-;N-(4-chlorophenyl)-2-(2,4-dichlorophenyl)prop-2-enamide;CHEMBL37715;DTXSID40148697

Suppliers and Price of Benzeneacetamide, 2,4-dichloro-N-(4-chlorophenyl)-a-methylene-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of Benzeneacetamide, 2,4-dichloro-N-(4-chlorophenyl)-a-methylene-

Chemical Property:

Vapor Pressure:6.25E-11mmHg at 25°C
Boiling Point:520.4°Cat760mmHg
Flash Point:268.5°C
Density:1.407g/cm³
XLogP3:5.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:324.982797
Heavy Atom Count:20
Complexity:366

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=C(C1=C(C=C(C=C1)Cl)Cl)C(=O)NC2=CC=C(C=C2)Cl

Technology Process of Benzeneacetamide, 2,4-dichloro-N-(4-chlorophenyl)-a-methylene-

There total 4 articles about Benzeneacetamide, 2,4-dichloro-N-(4-chlorophenyl)-a-methylene- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 106-47-8
4-chloro-aniline

: 108664-85-3
2-(2,4-Dichloro-phenyl)-acryloyl chloride

: 108664-50-2
2-(2,4-dichlorophenyl)-4'-chloroacrylanilide

Guidance literature:: With triethylamine; In dichloromethane; for 0.25h; Ambient temperature;
DOI:10.1021/jm00391a037

Reference yield:

: 6306-60-1
2,4-Dichlorophenylacetonitrile

: 108664-50-2
2-(2,4-dichlorophenyl)-4'-chloroacrylanilide

Guidance literature:: Multi-step reaction with 4 steps

1: 64 percent / Ac₂O / 2.5 h / 70 °C

2: 85 percent / 98percent H₂SO₄ / H₂O / 15 h / 130 °C

3: SOCl₂ / 0.5 h / 50 °C

4: 31 percent / Et₃N / CH₂Cl₂ / 0.25 h / Ambient temperature

With thionyl chloride; sulfuric acid; acetic anhydride; triethylamine; In dichloromethane; water;
DOI:10.1021/jm00391a037

Reference yield:

: 26923-38-6
2-(2,4-Dichloro-phenyl)-acrylonitrile

: 108664-50-2
2-(2,4-dichlorophenyl)-4'-chloroacrylanilide

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / 98percent H₂SO₄ / H₂O / 15 h / 130 °C

2: SOCl₂ / 0.5 h / 50 °C

3: 31 percent / Et₃N / CH₂Cl₂ / 0.25 h / Ambient temperature

With thionyl chloride; sulfuric acid; triethylamine; In dichloromethane; water;
DOI:10.1021/jm00391a037