Cobalt, hexacarbonyl(mu-((1,2-eta:1,2-eta)-1-propynylbenzene))di-, (Co-Co)

Base Information

Chemical Name:Cobalt, hexacarbonyl(mu-((1,2-eta:1,2-eta)-1-propynylbenzene))di-, (Co-Co)
CAS No.:53556-74-4
Molecular Formula:C₁₅H₈Co₂O₆
Molecular Weight:402.211
Hs Code.:
Mol file:53556-74-4.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cobalt, hexacarbonyl(mu-((1,2-eta:1,2-eta)-1-propynylbenzene))di-, (Co-Co)

Chemical Property:

Purity/Quality:

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MSDS Files:: SDS file from LookChem

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Technology Process of Cobalt, hexacarbonyl(mu-((1,2-eta:1,2-eta)-1-propynylbenzene))di-, (Co-Co)

There total 10 articles about Cobalt, hexacarbonyl(mu-((1,2-eta:1,2-eta)-1-propynylbenzene))di-, (Co-Co) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 673-32-5
1-Phenylprop-1-yne

: dicobalt octacarbonyl

: 53556-74-4
cobalt(carbonyl)3(μ-PhC2Me)cobalt(carbonyl)3

Guidance literature:: In toluene; byproducts: C27H24; inert atmosphere; excess of alkyne, refluxing for 15 min; filtration, volume reduction (reduced pressure), TLC (SiO2, light petroleum/Et2O); elem.anal.;
DOI:10.1016/0020-1693(94)04169-V

Reference yield: 55.0%

: 673-32-5
1-Phenylprop-1-yne

: 15226-74-1,61091-28-9,61117-58-6
dicobalt octacarbonyl

: 53556-74-4
cobalt(carbonyl)3(μ-PhC2Me)cobalt(carbonyl)3

Guidance literature:: In not given; reacting Co2(CO)8 soln. with alkyne until CO formation is completed; room temp.; under N2;
DOI:10.1016/S0022-328X(00)84714-2

Reference yield: 52.0%

: 111635-09-7
(carbonyl)3cobalt(μ-PhC2CH2(iron)(carbonyl)2Cp)cobalt(carbonyl)3

: 76-05-1
trifluoroacetic acid

: 53556-74-4
cobalt(carbonyl)3(μ-PhC2Me)cobalt(carbonyl)3

: 37048-23-0
[Fe(η-C5H5)(CO)2(O2CCF3)]

Guidance literature:: In dichloromethane; Addn. of CF3CO2H to soln. of trinuclear FeCo2-complex under inert gas with stirring at room temp., stirring (18 h).; Filtn. of a purple solid, trituration with acetone, filtn., concg. of red-brown filtrate yields iron-complex. Column chromy. (Al2O3, petroleum ether) of the first filtrate yields the dinuclear Co2-complex and unreacted trinuclear complex.;