(carbonyl)3cobalt(μ-PhC2CH2(iron)(carbonyl)2Cp)cobalt(carbonyl)3

Base Information

Chemical Name:(carbonyl)3cobalt(μ-PhC2CH2(iron)(carbonyl)2Cp)cobalt(carbonyl)3
CAS No.:111635-09-7
Molecular Formula:C₂₂H₁₂Co₂FeO₈
Molecular Weight:578.166
Hs Code.:

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Chemical Property of (carbonyl)3cobalt(μ-PhC2CH2(iron)(carbonyl)2Cp)cobalt(carbonyl)3

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Technology Process of (carbonyl)3cobalt(μ-PhC2CH2(iron)(carbonyl)2Cp)cobalt(carbonyl)3

There total 1 articles about (carbonyl)3cobalt(μ-PhC2CH2(iron)(carbonyl)2Cp)cobalt(carbonyl)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 15226-74-1,61091-28-9,61117-58-6
dicobalt octacarbonyl

: cyclopentadienyl(3-phenyl-2-propynyl)dicarbonyliron

: 111635-09-7
(carbonyl)3cobalt(μ-PhC2CH2(iron)(carbonyl)2Cp)cobalt(carbonyl)3

Guidance literature:: In pentane; Addn. of iron complex soln. to Co2(CO)8 soln. under inert gas with stirring over 15 min, gas is evolved color of mixt. changes from orange to dark purple, stirring (1 h).; Evapn. in vac., yields purple cryst. residue, column chromy. (Al2O3, pentane) gives small pink band of unidentified material then a green band which is collected, evapn. to dryness, elem. anal.;

Reference yield: 52.0%

: 111635-09-7
(carbonyl)3cobalt(μ-PhC2CH2(iron)(carbonyl)2Cp)cobalt(carbonyl)3

: 76-05-1
trifluoroacetic acid

: 53556-74-4
cobalt(carbonyl)3(μ-PhC2Me)cobalt(carbonyl)3

: 37048-23-0
[Fe(η-C5H5)(CO)2(O2CCF3)]

Guidance literature:: In dichloromethane; Addn. of CF3CO2H to soln. of trinuclear FeCo2-complex under inert gas with stirring at room temp., stirring (18 h).; Filtn. of a purple solid, trituration with acetone, filtn., concg. of red-brown filtrate yields iron-complex. Column chromy. (Al2O3, petroleum ether) of the first filtrate yields the dinuclear Co2-complex and unreacted trinuclear complex.;