4-acetyl-4-(prop-1-en-2-yl)heptanedinitrile

Base Information

Chemical Name:4-acetyl-4-(prop-1-en-2-yl)heptanedinitrile
CAS No.:16400-79-6
Molecular Formula:C₁₂H₁₆N₂O
Molecular Weight:204.272
Hs Code.:

Synonyms:Heptanedinitrile,4-acetyl-4-isopropenyl- (6CI,7CI,8CI); NSC 68485; g-Acetal-g-isopropenylpimelonitrile

Suppliers and Price of 4-acetyl-4-(prop-1-en-2-yl)heptanedinitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 4-acetyl-4-(prop-1-en-2-yl)heptanedinitrile

Chemical Property:

Vapor Pressure:1.08E-06mmHg at 25°C
Boiling Point:402.6°Cat760mmHg
Flash Point:197.3°C
Density:0.994g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-acetyl-4-(prop-1-en-2-yl)heptanedinitrile

There total 6 articles about 4-acetyl-4-(prop-1-en-2-yl)heptanedinitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 141-79-7
4-methyl-pent-3-en-2-one

: 107-13-1,25014-41-9
acrylonitrile

: 16400-79-6
4-acetyl-4-(prop-1-en-2-yl)heptanedinitrile

Guidance literature:: With potassium hydroxide; In methanol; tert-butyl alcohol; at 20 ℃; for 17h;
DOI:10.1002/chem.201901208

Reference yield:

: 89188-54-5
4-acetyl-5-methyl-hex-4-enenitrile

: 107-13-1,25014-41-9
acrylonitrile

: 16400-79-6
4-acetyl-4-(prop-1-en-2-yl)heptanedinitrile

Guidance literature:: With N-benzyl-trimethylammonium hydroxide; tert-butyl alcohol; at 10 - 15 ℃;
DOI:10.1021/ja01241a007

Reference yield:

: 141-79-7
4-methyl-pent-3-en-2-one

: 16400-79-6
4-acetyl-4-(prop-1-en-2-yl)heptanedinitrile

Guidance literature:: Multi-step reaction with 2 steps

1: trimethylbenzylammonium hydroxide; tert-butyl alcohol / 5 - 10 °C

2: trimethylbenzylammonium hydroxide; tert-butyl alcohol / 10 - 15 °C

With N-benzyl-trimethylammonium hydroxide; tert-butyl alcohol;
DOI:10.1021/ja01241a007