5-Phenyl-o-anisidine

Base Information

Chemical Name:5-Phenyl-o-anisidine
CAS No.:39811-17-1
Molecular Formula:C13H13NO
Molecular Weight:199.252
Hs Code.:29222910
European Community (EC) Number:254-639-7
UNII:FLC6AV3B78
DSSTox Substance ID:DTXSID70192880
Nikkaji Number:J236.616I
Wikidata:Q83065556
Mol file:39811-17-1.mol

Synonyms:5-Phenyl-o-anisidine;39811-17-1;3-Amino-4-methoxybiphenyl;4-Methoxy-[1,1'-biphenyl]-3-amine;2-Methoxy-5-phenylaniline;2-Amino-4-phenylanisole;4-methoxybiphenyl-3-amine;EINECS 254-639-7;FLC6AV3B78;(1,1'-Biphenyl)-3-amine, 4-methoxy-;[1,1'-Biphenyl]-3-amine, 4-methoxy-;EC 254-639-7;5-phenyl-2-anisidine;UNII-FLC6AV3B78;3-amino-4-methoxy-biphenyl;BIDD:GT0535;SCHEMBL330530;5-Phenyl-o-anisidine, >=98%;DTXSID70192880;4-methoxy(1,1'-biphenyl)-3-amine;MFCD00007790;AKOS005357771;FS-4467;4-Methoxy[1,1'-biphenyl]-3-amine #;A0958;CS-0168101;FT-0614985;D88361;EN300-1142275;A824742;J-511618

Suppliers and Price of 5-Phenyl-o-anisidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
5-Phenyl-o-anisidine
50mg
$ 45.00

TCI Chemical
3-Amino-4-methoxybiphenyl >98.0%(T)
5g
$ 98.00

TCI Chemical
3-Amino-4-methoxybiphenyl >98.0%(T)
25g
$ 293.00

SynQuest Laboratories
5-Phenyl-o-anisidine 99%
5 g
$ 187.00

SynQuest Laboratories
5-Phenyl-o-anisidine 99%
1 g
$ 79.00

Sigma-Aldrich
5-Phenyl-o-anisidine ≥98%
1g
$ 37.90

American Custom Chemicals Corporation
2-METHOXY-5-PHENYLANILINE 95.00%
5G
$ 883.58

Alichem
3-Amino-4-methoxybiphenyl
1g
$ 1534.70

Alichem
3-Amino-4-methoxybiphenyl
500mg
$ 815.00

Alichem
3-Amino-4-methoxybiphenyl
250mg
$ 475.20

Total 28 raw suppliers

Chemical Property of 5-Phenyl-o-anisidine

Chemical Property:

Appearance/Colour:brown coarse powder
Vapor Pressure:0.000103mmHg at 25°C
Melting Point:82-83 °C(lit.)
Refractive Index:1.553
Boiling Point:364.9 °C at 760 mmHg
PKA:4.28±0.10(Predicted)
Flash Point:186.3 °C
PSA：35.25000
Density:1.1 g/cm³
LogP:3.52560
Storage Temp.:Keep in dark place,Inert atmosphere,Room temperature
Solubility.:slightly sol. in Methanol
XLogP3:3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:199.099714038
Heavy Atom Count:15
Complexity:189

Purity/Quality:

99.9% ^*data from raw suppliers

5-Phenyl-o-anisidine ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 26-37/39-24/25

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)C2=CC=CC=C2)N
Uses 5-Phenyl-o-anisidine (2-Methoxy-5-phenylaniline) was used in the synthesis of 2,4-diamino-5-methyl-6-substituted-pyrido[2,3-d]pyrimidines.

Technology Process of 5-Phenyl-o-anisidine

There total 14 articles about 5-Phenyl-o-anisidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 15854-73-6
3-nitro-4-methoxybiphenyl

: 39811-17-1
5-phenyl-O-anisidine

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; for 8h;

Reference yield: 91.0%

: 77422-75-4
C₂₀H₁₉N₃OS

: 39811-17-1
5-phenyl-O-anisidine

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; methanol; water;
DOI:10.1021/ja00399a089

Reference yield: 86.0%

: 613-37-6
4-methoxylbiphenyl

: 39811-17-1
5-phenyl-O-anisidine

Guidance literature:: 4-methoxylbiphenyl; With (TMP)2Cu(CN)Li₂; In tetrahydrofuran; at -78 - 0 ℃; for 2h; Inert atmosphere; Schlenk technique;

With N-benzyloxyamine; In tetrahydrofuran; at -78 - 20 ℃; for 0.5h; regioselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1021/jacs.6b03855