10-Methoxyacenaphtho(1,2-b)quinoline

Base Information

• Chemical Name: 10-Methoxyacenaphtho(1,2-b)quinoline
• CAS No.: 132297-89-3
• Molecular Formula: C20H13NO
• Molecular Weight: 283.329
• UNII: SLA64HD7B9
• DSSTox Substance ID: DTXSID20157464
• Wikidata: Q83025603
• Mol file: 132297-89-3.mol

Synonyms:132297-89-3;10-Methoxyacenaphtho(1,2-b)quinoline;10-METHOXYACENAPHTHO[1,2-B]QUINOLINE;CCRIS 6580;Acenaphtho[1,2-b]quinoline,10-methoxy-;10-Methoxy-acenaphtho(1,2-b)quinoline;SLA64HD7B9;DTXSID20157464;Acenaphtho[1,2-b]quinoline, 10-methoxy-

Chemical Property of 10-Methoxyacenaphtho(1,2-b)quinoline

Chemical Property:

• Vapor Pressure: 6.51E-10mmHg at 25°C
• Refractive Index: 1.847
• Boiling Point: 507.3 °C at 760 mmHg
• Flash Point: 179.8 °C
• Density: 1.328 g/cm³
• XLogP3: 4.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 283.099714038
• Heavy Atom Count: 22
• Complexity: 424

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC2=CC3=C(C4=CC=CC5=C4C3=CC=C5)N=C2C=C1

Technology Process of 10-Methoxyacenaphtho(1,2-b)quinoline

There total 3 articles about 10-Methoxyacenaphtho(1,2-b)quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

1-((p-methoxyphenyl)amino)-2-(((p-methoxyphenyl)imino)methyl)acenaphthylene hydrochloride (132297-88-2) → 10-methoxyacenaphtho<1,2-b>quinoline (132297-89-3)

Guidance literature:

at 225 - 230 ℃;

DOI:10.1021/jo00006a063

Reference yield:

2-chloroacenaphthylene-1-carbaldehyde (13152-84-6) → 10-methoxyacenaphtho<1,2-b>quinoline (132297-89-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 97 percent / 2 N HCl / ethanol / 3 h / Ambient temperature

2: 52 percent / 225 - 230 °C

With hydrogenchloride; In ethanol;

DOI:10.1021/jo00006a063

Reference yield:

4-methoxy-aniline (104-94-9) → 10-methoxyacenaphtho<1,2-b>quinoline (132297-89-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 97 percent / 2 N HCl / ethanol / 3 h / Ambient temperature

2: 52 percent / 225 - 230 °C

With hydrogenchloride; In ethanol;

DOI:10.1021/jo00006a063

upstream raw materials:

1-((p-methoxyphenyl)amino)-2-(((p-methoxyphenyl)imino)methyl)acenaphthylene hydrochloride

2-chloroacenaphthylene-1-carbaldehyde

4-methoxy-aniline

Refernces