Methyl 3-(3,4-dimethoxyphenyl)oxirane-2-carboxylate

Base Information

Chemical Name:Methyl 3-(3,4-dimethoxyphenyl)oxirane-2-carboxylate
CAS No.:39829-15-7
Molecular Formula:C12H14O5
Molecular Weight:238.24
Hs Code.:
NSC Number:107450
DSSTox Substance ID:DTXSID30296075
Nikkaji Number:J3.492.910F
Mol file:39829-15-7.mol

Synonyms:39829-15-7;methyl 3-(3,4-dimethoxyphenyl)oxirane-2-carboxylate;NSC107450;SCHEMBL9692284;DTXSID30296075;NSC-107450

Suppliers and Price of Methyl 3-(3,4-dimethoxyphenyl)oxirane-2-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of Methyl 3-(3,4-dimethoxyphenyl)oxirane-2-carboxylate

Chemical Property:

Vapor Pressure:0.000295mmHg at 25°C
Boiling Point:321.6°Cat760mmHg
Flash Point:140.1°C
Density:1.227g/cm³
XLogP3:1.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:5
Exact Mass:238.08412354
Heavy Atom Count:17
Complexity:280

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)C2C(O2)C(=O)OC)OC

Technology Process of Methyl 3-(3,4-dimethoxyphenyl)oxirane-2-carboxylate

There total 4 articles about Methyl 3-(3,4-dimethoxyphenyl)oxirane-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 96-34-4
methyl chloroacetate

: 39829-15-7
methyl 3-(3,4-dimethoxyphenyl)oxirane-2-carboxylate

Guidance literature:: With sodium methylate; In methanol; -5 deg C, 2 h then 20 deg C, 3 h;
DOI:10.1016/S0957-4166(00)82268-5

Reference yield:

: 14737-89-4
3,4-dimethoxy-trans-cinnamic acid

: 39829-15-7
methyl 3-(3,4-dimethoxyphenyl)oxirane-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: H₂SO₄

2: m-chloroperbenzoic acid, sodium bicarbonate / CH₂Cl₂; H₂O / 24 h / Heating

With sulfuric acid; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; water;
DOI:10.1080/00397919608003584

Reference yield:

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 39829-15-7
methyl 3-(3,4-dimethoxyphenyl)oxirane-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

2: H₂SO₄

3: m-chloroperbenzoic acid, sodium bicarbonate / CH₂Cl₂; H₂O / 24 h / Heating

With sulfuric acid; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; water;
DOI:10.1080/00397919608003584