2-(phenoxymethyl)-1H-benzimidazole hydrochloride

Base Information

• Chemical Name: 2-(phenoxymethyl)-1H-benzimidazole hydrochloride
• CAS No.: 6637-29-2
• Molecular Formula: C14H12N2O
• Molecular Weight: 224.262
• Hs Code.: 2933990090
• Mol file: 6637-29-2.mol

Synonyms:Benzimidazole,2-(phenoxymethyl)- (8CI);2-(Phenoxymethyl)-1H-benzimidazole;2-(Phenoxymethyl)benzimidazole;NSC 52089;

Chemical Property of 2-(phenoxymethyl)-1H-benzimidazole hydrochloride

Chemical Property:

• Vapor Pressure: 1.78E-08mmHg at 25°C
• Refractive Index: 1.677
• Boiling Point: 467.7 °C at 760 mmHg
• Flash Point: 167.2 °C
• PSA: 37.91000
• Density: 1.247 g/cm³
• LogP: 3.14190

Purity/Quality:

97% ^*data from raw suppliers

2-(phenoxymethyl)-1H-benzimidazole ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(phenoxymethyl)-1H-benzimidazole hydrochloride

There total 3 articles about 2-(phenoxymethyl)-1H-benzimidazole hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

1,2-diamino-benzene (95-54-5) + 2-phenoxyacetic acid (122-59-8) → 2-(phenoxymethyl)-1H-benzimidazole (6637-29-2)

Guidance literature:

With trimethylsilyl polyphosphate ester; at 100 ℃; for 2.5h;

DOI:10.1016/j.ejmech.2003.11.014

Reference yield: 65.0%

1H-benzimidazole-2-sulfonic acid (40828-54-4) + 2-phenoxyacetic acid (122-59-8) → 2-(phenoxymethyl)-1H-benzimidazole (6637-29-2)

Guidance literature:

With ammonium persulfate; silver nitrate; In water; acetonitrile;

DOI:10.1007/BF00505976

Reference yield:

→ 2-(phenoxymethyl)-1H-benzimidazole (6637-29-2)

Guidance literature:

/BRN= 124251/;

upstream raw materials:

1H-benzimidazole-2-sulfonic acid

2-phenoxyacetic acid

1,2-diamino-benzene

Downstream raw materials:

C₂₁H₂₅ClN₂O

C₂₂H₂₇ClN₂O

C₂₃H₂₉ClN₂O

C₁₉H₂₁ClN₂O

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