Lutetate(1-),bis[29H,31H-phthalocyaninato(2-)-kN29,kN30,kN31,kN32]-, hydrogen (1:1), (SA-8-11''22''1'1'''2'2''')-

Base Information

• Chemical Name: Lutetate(1-),bis[29H,31H-phthalocyaninato(2-)-kN29,kN30,kN31,kN32]-, hydrogen (1:1), (SA-8-11''22''1'1'''2'2''')-
• CAS No.: 12369-74-3
• Molecular Formula: C64H32 Lu N16 . H
• Molecular Weight: 1201.04
• Mol file: 12369-74-3.mol

Synonyms:Lutetate(1-),bis[29H,31H-phthalocyaninato(2-)-N29,N30,N31,N32]-, hydrogen,(SA-8-11''22''1'1'''2'2''')-; Lutetate(1-), bis[29H,31H-phthalocyaninato(2-)-kN29,kN30,kN31,kN32]-, hydrogen,(SA-8-11''22''1'1'''2'2''')- (9CI); Lutetate(1-), bis[phthalocyaninato(2-)]-,hydrogen (8CI); 29H,31H-Phthalocyanine, lutetate(1-) deriv.;29H,31H-Phthalocyanine, lutetium complex; Hydrogenbis(phthalocyaninato)lutetate(1-); Hydrogen bis(phthalocyaninato)lutetium;Lutetium diphthalocyanine

Chemical Property of Lutetate(1-),bis[29H,31H-phthalocyaninato(2-)-kN29,kN30,kN31,kN32]-, hydrogen (1:1), (SA-8-11''22''1'1'''2'2''')-

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Lutetate(1-),bis[29H,31H-phthalocyaninato(2-)-kN29,kN30,kN31,kN32]-, hydrogen (1:1), (SA-8-11''22''1'1'''2'2''')-

There total 3 articles about Lutetate(1-),bis[29H,31H-phthalocyaninato(2-)-kN29,kN30,kN31,kN32]-, hydrogen (1:1), (SA-8-11''22''1'1'''2'2''')- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

{bis(phthalocyaninato)lutetium(III)}{Na.cntnd.18-crown-6} (112816-38-3) → bis(phthalocyaninato)lutetium(III)H (12369-74-3)

Guidance literature:

In methanol; chlorobenzene; MeOH added to soln. of raw Lu-complex;; concn. (vacuum); addn. of pentane; elem. anal.;;

Reference yield:

lutetium diphthalocyanine (79079-35-9) → bis(phthalocyaninato)lutetium(III)H (12369-74-3)

Guidance literature:

In methanol; N,N-dimethyl-formamide; passing alumina column (DMF/MeOH);

DOI:10.1246/bcsj.65.250

Reference yield:

phthalonitrile (91-15-6) + lutetium(III) acetate → bis(phthalocyaninato)lutetium(III)H (12369-74-3)

Guidance literature:

In melt; 1.5 h at 280-290°C; solidification; dissolving in DMF; filtration; chromy. (aluminium oxide, methanol eluent);

upstream raw materials:

phthalonitrile

{bis(phthalocyaninato)lutetium(III)}{Na_.cntnd.18-crown-6}

lutetium diphthalocyanine

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