5-Nitro-2-furancarboxylic acid 2-(2H-1,4-benzoxazin-3-yl)hydrazide

Base Information

Chemical Name:5-Nitro-2-furancarboxylic acid 2-(2H-1,4-benzoxazin-3-yl)hydrazide
CAS No.:78959-38-3
Molecular Formula:C₁₃H₁₀N₄O₅
Molecular Weight:302.246
Hs Code.:
DSSTox Substance ID:DTXSID201000158
Wikidata:Q82993584
Mol file:78959-38-3.mol

Synonyms:BRN 4565665;5-Nitro-2-furancarboxylic acid 2-(2H-1,4-benzoxazin-3-yl)hydrazide;2-Furancarboxylic acid, 5-nitro-, 2-(2H-1,4-benzoxazin-3-yl)hydrazide;DTXSID201000158;LS-70175;N-(2H-1,4-Benzoxazin-3-yl)-5-nitrofuran-2-carbohydrazonic acid

Suppliers and Price of 5-Nitro-2-furancarboxylic acid 2-(2H-1,4-benzoxazin-3-yl)hydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-FURANCARBOXYLIC ACID, 5-NITRO-, 2-(2H-1,4-BENZOXAZIN-3-YL)HYDRAZIDE 95.00%
5MG
$ 496.84

Total 3 raw suppliers

Chemical Property of 5-Nitro-2-furancarboxylic acid 2-(2H-1,4-benzoxazin-3-yl)hydrazide

Chemical Property:

PSA：125.17000
Density:1.62g/cm3
LogP:2.46930
XLogP3:1.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:3
Exact Mass:302.06511943
Heavy Atom Count:22
Complexity:478

Purity/Quality:: 2-FURANCARBOXYLIC ACID, 5-NITRO-, 2-(2H-1,4-BENZOXAZIN-3-YL)HYDRAZIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C(=NC2=CC=CC=C2O1)NNC(=O)C3=CC=C(O3)[N+](=O)[O-]

Technology Process of 5-Nitro-2-furancarboxylic acid 2-(2H-1,4-benzoxazin-3-yl)hydrazide

There total 3 articles about 5-Nitro-2-furancarboxylic acid 2-(2H-1,4-benzoxazin-3-yl)hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 21744-76-3
3-methylthio-2H-1,4-benzoxazine

: 5469-78-3
5-nitrofuran-2-carbohydrazide

: 78959-38-3
5-nitro-2-furoic acid 2-(2H-1,4-benzoxazin-3-yl)hydrazide

Guidance literature:: In ethanol; Ambient temperature;

Reference yield:

: 14183-51-8
2H-1,4-benzoxazin-3(4H)-thione

: 78959-38-3
5-nitro-2-furoic acid 2-(2H-1,4-benzoxazin-3-yl)hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / acetone / 8 h / Heating

2: 70 percent / ethanol / Ambient temperature

With potassium carbonate; In ethanol; acetone;

Reference yield:

: 5466-88-6
3,4-dihydro-3-oxo-2H-1,4-benzoxazine

: 78959-38-3
5-nitro-2-furoic acid 2-(2H-1,4-benzoxazin-3-yl)hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / P₂S₅/Et₃N / acetonitrile

2: K₂CO₃ / acetone / 8 h / Heating

3: 70 percent / ethanol / Ambient temperature

With tetraphosphorus decasulfide; potassium carbonate; triethylamine; In ethanol; acetone; acetonitrile;