MD 780232

Base Information

Chemical Name:MD 780232
CAS No.:73422-62-5
Molecular Formula:C₁₁H₁₃NO₄
Molecular Weight:223.229
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of MD 780232

Chemical Property:

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Technology Process of MD 780232

There total 3 articles about MD 780232 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: (R)-3-(4-(benzyloxy)phenyl)-5-(methoxymethyl)oxazolidin-2-one

: 73422-62-5,135605-66-2
3-(4-hydroxyphenyl)-5-(methoxymethyl)oxazolidin-2-one

Guidance literature:: With 5%-palladium/activated carbon; hydrogen; In ethanol; dichloromethane; at 20 ℃; for 12h;
DOI:10.1039/c2cc32757k

Reference yield:

: 693830-78-3
methyl (4-(benzyloxy)phenyl)carbamate

: 73422-62-5,135605-66-2
3-(4-hydroxyphenyl)-5-(methoxymethyl)oxazolidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 155 °C / Inert atmosphere

2: 5%-palladium/activated carbon; hydrogen / ethanol; dichloromethane / 12 h / 20 °C

With 5%-palladium/activated carbon; hydrogen; potassium carbonate; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2cc32757k

Reference yield:

: 51388-20-6
4-benzyloxyaniline hydrochloride

: 73422-62-5,135605-66-2
3-(4-hydroxyphenyl)-5-(methoxymethyl)oxazolidin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 8 h / 20 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 3 h / 155 °C / Inert atmosphere

3: 5%-palladium/activated carbon; hydrogen / ethanol; dichloromethane / 12 h / 20 °C

With 5%-palladium/activated carbon; hydrogen; potassium carbonate; triethylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2cc32757k