4-Nitrobenzaldehyde hydrazone

Base Information

• Chemical Name: 4-Nitrobenzaldehyde hydrazone
• CAS No.: 6310-10-7
• Molecular Formula: C7H7 N3 O2
• Molecular Weight: 165.151
• Hs Code.: 2928000090
• European Community (EC) Number: 228-631-9
• NSC Number: 43024
• ChEMBL ID: CHEMBL3415441
• Mol file: 6310-10-7.mol

Synonyms:4-Nitrobenzaldehyde hydrazone;CHEMBL3415441;4-NITROBENZALDEHYDE HYDRAZONE, 98;6310-10-7;SCHEMBL5881216;NSC43024;EINECS 228-631-9;BDBM50078678;NSC 43024;NSC-43024;AKOS002969579;(E)-(4-nitrophenyl)methylidenehydrazine;AI3-52015

Chemical Property of 4-Nitrobenzaldehyde hydrazone

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Melting Point: 135-137 °C(lit.)
• Boiling Point: 338.575°C at 760 mmHg
• Flash Point: 158.565°C
• PSA: 84.20000
• Density: 1.337g/cm³
• LogP: 2.11090
• XLogP3: 1.6
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 1
• Exact Mass: 165.053826475
• Heavy Atom Count: 12
• Complexity: 180

Purity/Quality:

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-37/39

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: C1=CC(=CC=C1C=NN)[N+](=O)[O-]
• Isomeric SMILES: C1=CC(=CC=C1/C=N/N)[N+](=O)[O-]

Technology Process of 4-Nitrobenzaldehyde hydrazone

There total 9 articles about 4-Nitrobenzaldehyde hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

4-nitrobenzaldehdye (555-16-8) → 4-nitrobenzaldehyde hydrazone (6310-10-7)

Guidance literature:

With hydrazine hydrate; at 100 ℃; for 6h; Sealed tube;

DOI:10.1021/jo401377a

Reference yield:

4-nitro-benzaldehyde dimethylhydrazone (10424-92-7) → 4-nitrobenzaldehyde hydrazone (6310-10-7)

Guidance literature:

With hydrazine; In ethanol; Heating;

DOI:10.1021/jo01341a008

Reference yield:

bis(4-nitrobenzyl)disulfide (39549-05-8) → 4-nitrobenzaldehyde hydrazone (6310-10-7)

Guidance literature:

With hydrazine hydrate; In ethanol; Heating;

upstream raw materials:

4-nitrobenzaldehdye

4-nitro-benzaldehyde dimethylhydrazone

bis(4-nitrobenzyl)disulfide

cyano-acetic acid-(4-nitro-benzylidenehydrazide)

Downstream raw materials:

N-benzylidene-N¹-(4-nitrobenylidene)-hydrazine

C₁₄H₁₁ClN₄O₃

3-{N'-[1-(4-Nitro-phenyl)-meth-(E)-ylidene]-hydrazinothiocarbonylsulfanyl}-propionic acid

1,2-bis(4-nitrobenzylidene)hydrazine