4-Nitrobenzaldehyde dimethylhydrazone

Base Information

• Chemical Name: 4-Nitrobenzaldehyde dimethylhydrazone
• CAS No.: 10424-92-7
• Molecular Formula: C9H11 N3 O2
• Molecular Weight: 193.205
• Hs Code.: 2928000090
• European Community (EC) Number: 634-631-3
• Mol file: 10424-92-7.mol

Synonyms:4-Nitrobenzaldehyde dimethylhydrazone;10424-92-7;Benzaldehyde, p-nitro-, dimethylhydrazone;BRN 2211200;N-methyl-N-[(E)-(4-nitrophenyl)methylideneamino]methanamine;1,1-Dimethyl-2-(4-nitrobenzylidene)hydrazine;4-07-00-00605 (Beilstein Handbook Reference);IPBHNKLEYSNEBU-JXMROGBWSA-N;CCG-42812;Benzaldehyde, 4-nitro-, dimethylhydrazone;LS-25118;4-nitrobenzalde-hyde N,N-dimethylhydrazone;SR-01000632781-1

Chemical Property of 4-Nitrobenzaldehyde dimethylhydrazone

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 342.1°Cat760mmHg
• Flash Point: 160.7°C
• PSA: 61.42000
• Density: 1.14g/cm³
• LogP: 2.01350
• XLogP3: 2.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 193.085126602
• Heavy Atom Count: 14
• Complexity: 215

Purity/Quality:

98%,99%, ^*data from raw suppliers

4-NITROBENZALDEHYDE DIMETHYLHYDRAZONE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)N=CC1=CC=C(C=C1)[N+](=O)[O-]
• Isomeric SMILES: CN(C)/N=C/C1=CC=C(C=C1)[N+](=O)[O-]

Technology Process of 4-Nitrobenzaldehyde dimethylhydrazone

There total 3 articles about 4-Nitrobenzaldehyde dimethylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

p-nitrobenzyl azide (17271-88-4) + N,N-Dimethylhydrazine (57-14-7) → 4-nitro-benzaldehyde dimethylhydrazone (10424-92-7)

Guidance literature:

iron(III) chloride; In acetonitrile; for 3h; Heating;

DOI:10.1021/jo000708w

Reference yield: 96.0%

4-nitrobenzaldehdye (555-16-8) + N,N-Dimethylhydrazine (57-14-7) → 4-nitro-benzaldehyde dimethylhydrazone (10424-92-7)

Guidance literature:

In methanol; at 20 ℃; for 2h;

Reference yield:

→ 4-nitro-benzaldehyde dimethylhydrazone (10424-92-7)

Guidance literature:

DOI:10.1021/jo01080a027

upstream raw materials:

4-nitrobenzaldehdye

N,N-Dimethylhydrazine

p-nitrobenzyl azide

Downstream raw materials:

4-nitrobenzaldehyde hydrazone

4-aminobenzaldehyde N,N-dimethylhydrazone

N-[2-(Dimethyl-hydrazono)-2-(4-nitro-phenyl)-acetyl]-methanesulfonamide

N,N-Dimethyl-N'-[1-(4-nitro-phenyl)-meth-(E)-ylidene]-hydrazine; hydrochloride