trans-2-Methoxy-4,5-methylenedioxycinnamaldehyde

Base Information

Chemical Name:trans-2-Methoxy-4,5-methylenedioxycinnamaldehyde
CAS No.:67323-02-8
Molecular Formula:C11H10O4
Molecular Weight:206.198
Hs Code.:
Nikkaji Number:J2.375.924A,J620.491K

Synonyms:67323-02-8;trans-2-Methoxy-4,5-methylenedioxycinnamaldehyde;(E)-3-(6-Methoxybenzo(1,3)dioxol-5-yl)prop-2-enal;3-(2-Methoxy-4,5-methylenedioxyphenyl)propenal;SCHEMBL23728286;3-(6-methoxy-1,3-dioxaindan-5-yl)prop-2-enal;EN300-1996766;(E)-3-(6-Methoxy-1,3-benzodioxol-5-yl)propenal

Suppliers and Price of trans-2-Methoxy-4,5-methylenedioxycinnamaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of trans-2-Methoxy-4,5-methylenedioxycinnamaldehyde

Chemical Property:

Vapor Pressure:3.61E-05mmHg at 25°C
Boiling Point:353.4°Cat760mmHg
Flash Point:158.8°C
Density:1.265g/cm³
XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:206.05790880
Heavy Atom Count:15
Complexity:251

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC2=C(C=C1C=CC=O)OCO2
Isomeric SMILES:COC1=CC2=C(C=C1/C=C/C=O)OCO2

Technology Process of trans-2-Methoxy-4,5-methylenedioxycinnamaldehyde

There total 5 articles about trans-2-Methoxy-4,5-methylenedioxycinnamaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 18607-93-7
1-allyl-2-methoxy-4,5-methylenedioxybenzene

: 67323-02-8
3-(2-Methoxy-4,5-methylendioxyphenyl)acrolein

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In water; 1,2-dichloro-ethane; for 24h; Reflux;
DOI:10.1002/cbdv.202100779

Reference yield:

: 533-31-3
Sesamol

: 67323-02-8
3-(2-Methoxy-4,5-methylendioxyphenyl)acrolein

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetone / 60 °C

2: N,N-dimethyl-aniline / 190 °C

3: potassium carbonate / acetone / 60 °C

4: 2,3-dicyano-5,6-dichloro-p-benzoquinone; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; 1,2-dichloro-ethane / 50 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In water; N,N-dimethyl-aniline; 1,2-dichloro-ethane; acetone;

Reference yield:

: 19202-22-3
O-allyl-sesamol

: 67323-02-8
3-(2-Methoxy-4,5-methylendioxyphenyl)acrolein

Guidance literature:: Multi-step reaction with 3 steps

1: N,N-dimethyl-aniline / 190 °C

2: potassium carbonate / acetone / 60 °C

3: 2,3-dicyano-5,6-dichloro-p-benzoquinone; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; 1,2-dichloro-ethane / 50 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In water; N,N-dimethyl-aniline; 1,2-dichloro-ethane; acetone;