Azacyclotetradecane

Base Information

Chemical Name:Azacyclotetradecane
CAS No.:295-18-1
Molecular Formula:C13H27 N
Molecular Weight:0
Hs Code.:
DSSTox Substance ID:DTXSID60454646
Nikkaji Number:J79.583F
Wikidata:Q82276294
Mol file:295-18-1.mol

Synonyms:Azacyclotetradecane;295-18-1;1-azacyclotetradecane;SCHEMBL82847;DTXSID60454646

Suppliers and Price of Azacyclotetradecane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of Azacyclotetradecane

Chemical Property:

PSA：12.03000
LogP:4.20950
XLogP3:4.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:197.214349865
Heavy Atom Count:14
Complexity:99.8

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCCCCCNCCCCCC1

Technology Process of Azacyclotetradecane

There total 6 articles about Azacyclotetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 7518-64-1
1-azacyclotetradecan-2-one

: 295-18-1
azacyclotetradecane

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 70 ℃; for 19h;
DOI:10.1021/ol991029e

Reference yield: 65.0%

: 1033235-36-7
N-benzyl-3-(p-chlorobenzenesulfonyl)azacyclotetradecane

: 295-18-1
azacyclotetradecane

Guidance literature:: With ammonia; sodium; In tetrahydrofuran; at -78 ℃; for 0.5h;
DOI:10.1021/jo800600a

Reference yield:

: 832-10-0
cyclotridecanone

: 295-18-1
azacyclotetradecane

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / NH₂OH*HCl; NaHCO₃ / methanol

2: 100 percent / P₂O₅; CH₃SO₃H

3: 60 percent / LiAlH₄ / tetrahydrofuran / Heating

With lithium aluminium tetrahydride; methanesulfonic acid; hydroxylamine hydrochloride; phosphorus pentoxide; sodium hydrogencarbonate; In tetrahydrofuran; methanol; 1: Condensation / 2: Rearrangement / 3: Reduction;
DOI:10.1016/S0040-4039(99)01016-3