2-Thiaspiro[3.5]nonane

Base Information

Chemical Name:2-Thiaspiro[3.5]nonane
CAS No.:185-11-5
Molecular Formula:C8H14S
Molecular Weight:142.2618
Hs Code.:
NSC Number:243159
DSSTox Substance ID:DTXSID60311422
Wikidata:Q82061090

Synonyms:2-Thiaspiro[3.5]nonane;185-11-5;NSC243159;SCHEMBL10477427;DTXSID60311422;NSC-243159

Suppliers and Price of 2-Thiaspiro[3.5]nonane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 9 raw suppliers

Chemical Property of 2-Thiaspiro[3.5]nonane

Chemical Property:

Vapor Pressure:0.141mmHg at 25°C
Boiling Point:223.8°Cat760mmHg
Flash Point:84.3°C
Density:1.03g/cm³
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:142.08162162
Heavy Atom Count:9
Complexity:97.1

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CCC2(CC1)CSC2

Technology Process of 2-Thiaspiro[3.5]nonane

There total 9 articles about 2-Thiaspiro[3.5]nonane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 176-72-7
4,4-pentamethylene-1,2-dithiolane

: 185-11-5
2-thiaspiro[3.5]nonane

Guidance literature:: In pentane; at 5 ℃; for 1.66667h; Irradiation;
DOI:10.1246/bcsj.53.1982

Reference yield:

: 22308-11-8
cyclohexane-1,1-diylbis(methylene)bis(4-methylbenzenesulfonate)

: 185-11-5
2-thiaspiro[3.5]nonane

Guidance literature:: With sodium sulfide; In N,N-dimethyl-formamide; at 20 - 100 ℃; Schlenk technique;
DOI:10.1039/c7cc08553b

Reference yield:

: 1139-13-5
diethyl cyclohexane-1,1-dicarboxylate

: 185-11-5
2-thiaspiro[3.5]nonane

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

2: pyridine / 0 - 20 °C / Schlenk technique

3: sodium sulfide / N,N-dimethyl-formamide / 20 - 100 °C / Schlenk technique

With pyridine; sodium sulfide; lithium aluminium tetrahydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c7cc08553b