benzyl N-[(E)-pyridin-2-ylmethylideneamino]carbamodithioate

Base Information

Chemical Name:benzyl N-[(E)-pyridin-2-ylmethylideneamino]carbamodithioate
CAS No.:66415-74-5
Molecular Formula:C₁₄H₁₃N₃S₂
Molecular Weight:287.409
Hs Code.:
NSC Number:295637

Synonyms:NSC295637;66415-74-5;NSC-295637

Suppliers and Price of benzyl N-[(E)-pyridin-2-ylmethylideneamino]carbamodithioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of benzyl N-[(E)-pyridin-2-ylmethylideneamino]carbamodithioate

Chemical Property:

Vapor Pressure:2.58E-08mmHg at 25°C
Boiling Point:450.7°Cat760mmHg
Flash Point:226.4°C
Density:1.2g/cm³
XLogP3:3.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:287.05508977
Heavy Atom Count:19
Complexity:301

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)CSC(=S)NN=CC2=CC=CC=N2
Isomeric SMILES:C1=CC=C(C=C1)CSC(=S)N/N=C/C2=CC=CC=N2

Technology Process of benzyl N-[(E)-pyridin-2-ylmethylideneamino]carbamodithioate

There total 1 articles about benzyl N-[(E)-pyridin-2-ylmethylideneamino]carbamodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.9%

: 1121-60-4
pyridine-2-carbaldehyde

: 13331-31-2
S-benzyldithiocarbazate

: 66415-74-5
S-benzyl-β-N-((2-pyridyl)-methylene)-dithiocarbazate

Guidance literature:: In ethanol; for 0.25h; Reflux;
DOI:10.1039/c2dt12387h

Reference yield: 94.0%

: 66415-74-5
S-benzyl-β-N-((2-pyridyl)-methylene)-dithiocarbazate

: 7646-85-7,24359-56-6
zinc(II) chloride

: [Zn((C₅H₄N)CHNNCSSCH₂C₆H₅)2]

Guidance literature:: In ethanol; ligand dissolved in boiling ethanol, soln. of ZnCl2 added (1:1); stored overnight, crystd., filtered off, washed (ethanol), dried (vac.),elem. anal.;
DOI:10.1016/S0277-5387(01)00817-8

Reference yield: 81.4%

: cadmium bromide tetrahydrate

: 66415-74-5
S-benzyl-β-N-((2-pyridyl)-methylene)-dithiocarbazate

: [Cd((C₅H₄N)CHNNCSSCH₂C₆H₅)Br]

Guidance literature:: In ethanol; ligand dissolved in boiling ethanol, soln. of CdBr2*2H2O added (1:1), stirred for 20 min; stored overnight, crystd., filtered off, washed (ethanol), dried (vac.),elem. anal.;
DOI:10.1016/S0277-5387(01)00817-8