(3R,4R)-3,4-Dihydrodibenz(c,h)acridine-3,4-diol

Base Information

Chemical Name:(3R,4R)-3,4-Dihydrodibenz(c,h)acridine-3,4-diol
CAS No.:93780-91-7
Molecular Formula:
Molecular Weight:
Hs Code.:
DSSTox Substance ID:DTXSID80917985
Wikidata:Q82889822

Synonyms:CCRIS 8830;93780-91-7;(3R,4R)-3,4-Dihydrodibenz(c,h)acridine-3,4-diol;Dibenz(c,h)acridine-3,4-diol, 3,4-dihydro-, (3R,4R)-;(3R,4R)-3,4-DIHYDRODIBENZ[C,H]ACRIDINE-3,4-DIOL;DTXSID80917985;3,4-dihydrodibenzo[c,h]acridine-3,4-diol

Suppliers and Price of (3R,4R)-3,4-Dihydrodibenz(c,h)acridine-3,4-diol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of (3R,4R)-3,4-Dihydrodibenz(c,h)acridine-3,4-diol

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:313.110278721
Heavy Atom Count:24
Complexity:506

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C=CC3=CC4=C(C5=C(C=C4)C(C(C=C5)O)O)N=C32
Isomeric SMILES:C1=CC=C2C(=C1)C=CC3=CC4=C(C5=C(C=C4)[C@H]([C@@H](C=C5)O)O)N=C32

Technology Process of (3R,4R)-3,4-Dihydrodibenz(c,h)acridine-3,4-diol

There total 21 articles about (3R,4R)-3,4-Dihydrodibenz(c,h)acridine-3,4-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 93716-08-6
trans-3,4-diacetoxy-3,4-dihydrodibenzacridine

: 76186-87-3,93716-09-7,93780-91-7,93780-92-8,104012-38-6
trans-3,4-dihydroxy-3,4-dihydro-dibenzoacridine

Guidance literature:: With ammonia; In tetrahydrofuran; methanol; for 4h; Ambient temperature;
DOI:10.1021/jo00201a019

Reference yield: 80.0%

: trans-3,4-dibenzoxy-3,4-dihydro-dibenzoacridine

: 76186-87-3,93716-09-7,93780-91-7,93780-92-8,104012-38-6
trans-3,4-dihydroxy-3,4-dihydro-dibenzoacridine

Guidance literature:: With ammonium hydroxide; In methanol;

Reference yield:

: 90-15-3
α-naphthol

: 76186-87-3,93716-09-7,93780-91-7,93780-92-8,104012-38-6
trans-3,4-dihydroxy-3,4-dihydro-dibenzoacridine

Guidance literature:: Multi-step reaction with 7 steps

1: 12.9 percent / 0.25 h / 250 °C

3: 88 percent / 25percent aq. NaOH / tetrahydrofuran; methanol / 5 h / Ambient temperature

4: 92 percent / pyridine / 24 h / Ambient temperature

5: 96 percent / NBS, AIBN / CCl₄ / 0.25 h / 60 - 62 °C

6: 66 percent / Li₂CO₃, LiF / hexamethylphosphoric acid triamide / 3 h / 85 - 90 °C

7: 93 percent / NH₃ / methanol; tetrahydrofuran / 4 h / Ambient temperature

With pyridine; sodium hydroxide; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); ammonia; lithium carbonate; lithium fluoride; In tetrahydrofuran; methanol; tetrachloromethane; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1021/jo00201a019